Technology Process of C21H26N2O4S
There total 4 articles about C21H26N2O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
camphor-10-sulfonic acid;
In
dichloromethane;
at 20 ℃;
for 0.166667h;
Inert atmosphere;
DOI:10.1021/ol203030a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: diisobutylaluminium hydride / toluene / 3 h / 0 °C / Inert atmosphere
2: N-Bromosuccinimide; triphenylphosphine / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere
3: tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / -78 - 20 °C / Inert atmosphere
4: camphor-10-sulfonic acid / dichloromethane / 0.17 h / 20 °C / Inert atmosphere
With
N-Bromosuccinimide; camphor-10-sulfonic acid; diisobutylaluminium hydride; triphenylphosphine;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol203030a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / -78 - 20 °C / Inert atmosphere
2: camphor-10-sulfonic acid / dichloromethane / 0.17 h / 20 °C / Inert atmosphere
With
camphor-10-sulfonic acid;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1021/ol203030a