C₃₂H₅₃NO₁₅

Base Information

Chemical Name:C₃₂H₅₃NO₁₅
CAS No.:1609184-34-0
Molecular Formula:C₃₂H₅₃NO₁₅
Molecular Weight:691.771
Hs Code.:

C<sub>32</sub>H<sub>53</sub>NO<sub>15</sub>

Synonyms:C₃₂H₅₃NO₁₅

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Chemical Property of C₃₂H₅₃NO₁₅

Chemical Property:

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Technology Process of C₃₂H₅₃NO₁₅

There total 16 articles about C₃₂H₅₃NO₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374760-30-1
C₄₀H₅₉NO₁₆

: 1609184-34-0
C₃₂H₅₃NO₁₅

Guidance literature:: C₄₀H₅₉NO₁₆; With methanol; sodium methylate; at 20 ℃;

With water; at 50 ℃; for 3h;

Reference yield:

: 1374760-20-9
C₁₆H₃₀O₄Si

: 1609184-34-0
C₃₂H₅₃NO₁₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: tetraethylammonium bromide / dichloromethane; N,N-dimethyl-formamide / 1 h / 20 °C / Molecular sieve; Inert atmosphere

1.2: 18 h / 20 °C / Inert atmosphere; Cooling with ice

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 15 h / 20 °C

3.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve

3.2: 2 h / 0 °C

4.1: methanol; sodium methylate / 2 h

5.1: triethylamine / acetonitrile / 1.33 h / 0 °C

6.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux

6.2: 20 °C

7.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-n-butyl-tin hydride / dichloromethane / 1 h / 20 °C

8.1: palladium 10% on activated carbon; hydrogen; acetic acid / water; 1,4-dioxane / 5 h / 20 °C / 1034.32 Torr

9.1: methanol; sodium methylate / 20 °C

9.2: 3 h / 50 °C

With methanol; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; tetraethylammonium bromide; tetrabutyl ammonium fluoride; hydrogen; tri-n-butyl-tin hydride; sodium methylate; di(n-butyl)tin oxide; acetic acid; triethylamine; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 127943-95-7
methyl (1R,3R)-3-(tert-butyldimethylsilyloxy)cyclohex-4-ene-1-carboxylate

: 1609184-34-0
C₃₂H₅₃NO₁₅

Guidance literature:: Multi-step reaction with 11 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / 0 °C / Inert atmosphere

2.2: 0.5 h / -20 °C / Inert atmosphere

3.1: tetraethylammonium bromide / dichloromethane; N,N-dimethyl-formamide / 1 h / 20 °C / Molecular sieve; Inert atmosphere

3.2: 18 h / 20 °C / Inert atmosphere; Cooling with ice

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 15 h / 20 °C

5.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve

5.2: 2 h / 0 °C

6.1: methanol; sodium methylate / 2 h

7.1: triethylamine / acetonitrile / 1.33 h / 0 °C

8.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux

8.2: 20 °C

9.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-n-butyl-tin hydride / dichloromethane / 1 h / 20 °C

10.1: palladium 10% on activated carbon; hydrogen; acetic acid / water; 1,4-dioxane / 5 h / 20 °C / 1034.32 Torr

11.1: methanol; sodium methylate / 20 °C

11.2: 3 h / 50 °C

With methanol; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; palladium 10% on activated carbon; tetraethylammonium bromide; tetrabutyl ammonium fluoride; hydrogen; tri-n-butyl-tin hydride; sodium methylate; di(n-butyl)tin oxide; acetic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; 1,4-dioxane; methanol; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;