(2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-sulfo-α-D-glucopyranosyl)-(1->4)-[(2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol)uronic acid]

Base Information

Chemical Name:(2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-sulfo-α-D-glucopyranosyl)-(1->4)-[(2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol)uronic acid]
CAS No.:1252259-02-1
Molecular Formula:C₄₈H₅₁N₃O₁₇S₂
Molecular Weight:1006.07
Hs Code.:

(2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-sulfo-α-D-glucopyranosyl)-(1->4)-[(2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol)uronic acid]

Synonyms:(2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-sulfo-α-D-glucopyranosyl)-(1->4)-[(2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol)uronic acid]

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Chemical Property of (2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-sulfo-α-D-glucopyranosyl)-(1->4)-[(2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol)uronic acid]

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Technology Process of (2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-sulfo-α-D-glucopyranosyl)-(1->4)-[(2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol)uronic acid]

There total 1 articles about (2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-sulfo-α-D-glucopyranosyl)-(1->4)-[(2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol)uronic acid] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1252027-52-3
(2-acetamido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-[tert-butyl (2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol)uronate]

: 1252259-02-1
(2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-sulfo-α-D-glucopyranosyl)-(1->4)-[(2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol)uronic acid]

Guidance literature:: (2-acetamido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-[tert-butyl (2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol)uronate]; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

With sulfur trioxide pyridine complex; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h;
DOI:10.1016/j.tet.2010.07.055

Reference yield: 73.0%

: 1252259-02-1
(2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-sulfo-α-D-glucopyranosyl)-(1->4)-[(2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol)uronic acid]

: C₄₂H₄₆N₂O₁₃S^(2-)*2Na⁽¹⁺⁾

Guidance literature:: (2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-sulfo-α-D-glucopyranosyl)-(1->4)-[(2,3-di-O-benzyl-1,5-dideoxy-1,5-imino-N-(4-nitro)benzenesulfonyl-L-iditol)uronic acid]; In methanol;

With thiophenol; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h; pH=8;
DOI:10.1016/j.tet.2010.07.055