3-hydroxy-4-((3-hydroxyphenylimino)methyl)phenyl 4-n-dodecyloxybenzoate

Base Information

Chemical Name:3-hydroxy-4-((3-hydroxyphenylimino)methyl)phenyl 4-n-dodecyloxybenzoate
CAS No.:1363408-10-9
Molecular Formula:C₃₂H₃₉NO₅
Molecular Weight:517.665
Hs Code.:

Synonyms:3-hydroxy-4-((3-hydroxyphenylimino)methyl)phenyl 4-n-dodecyloxybenzoate

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Chemical Property of 3-hydroxy-4-((3-hydroxyphenylimino)methyl)phenyl 4-n-dodecyloxybenzoate

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Technology Process of 3-hydroxy-4-((3-hydroxyphenylimino)methyl)phenyl 4-n-dodecyloxybenzoate

There total 3 articles about 3-hydroxy-4-((3-hydroxyphenylimino)methyl)phenyl 4-n-dodecyloxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 868620-29-5
4-(2`hydroxy-4`-dodecylhydroxybenzoylhydroxy)benzaldehyde

: 591-27-5
m-Hydroxyaniline

: 1363408-10-9
3-hydroxy-4-((3-hydroxyphenylimino)methyl)phenyl 4-n-dodecyloxybenzoate

Guidance literature:: With acetic acid; In ethanol; at 20 ℃; for 24h;
DOI:10.3762/bjoc.8.15

Reference yield:

: 2312-15-4
p-dodecyloxybenzoic acid

: 1363408-10-9
3-hydroxy-4-((3-hydroxyphenylimino)methyl)phenyl 4-n-dodecyloxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; oxalyl dichloride / dichloromethane / 2 h / Reflux

2: dmap; triethylamine / toluene / 16 h / 20 - 65 °C

3: acetic acid / ethanol / 24 h / 20 °C

With pyridine; dmap; oxalyl dichloride; acetic acid; triethylamine; In ethanol; dichloromethane; toluene;
DOI:10.3762/bjoc.8.15

Reference yield:

: 50909-50-7
4-dodecyloxybenzoyl chloride

: 1363408-10-9
3-hydroxy-4-((3-hydroxyphenylimino)methyl)phenyl 4-n-dodecyloxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / toluene / 16 h / 20 - 65 °C

2: acetic acid / ethanol / 24 h / 20 °C

With dmap; acetic acid; triethylamine; In ethanol; toluene;
DOI:10.3762/bjoc.8.15