methyl 12-cyclohexyl-6-oxo-6,7-dihydro-5H-thieno[2',3':4,5]pyrrolo[1,2-d][1,4]benzodiazepine-10-carboxylate

Base Information

Chemical Name:methyl 12-cyclohexyl-6-oxo-6,7-dihydro-5H-thieno[2',3':4,5]pyrrolo[1,2-d][1,4]benzodiazepine-10-carboxylate
CAS No.:886972-70-9
Molecular Formula:C₂₂H₂₂N₂O₃S
Molecular Weight:394.494
Hs Code.:

Synonyms:methyl 12-cyclohexyl-6-oxo-6,7-dihydro-5H-thieno[2',3':4,5]pyrrolo[1,2-d][1,4]benzodiazepine-10-carboxylate

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Chemical Property of methyl 12-cyclohexyl-6-oxo-6,7-dihydro-5H-thieno[2',3':4,5]pyrrolo[1,2-d][1,4]benzodiazepine-10-carboxylate

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Technology Process of methyl 12-cyclohexyl-6-oxo-6,7-dihydro-5H-thieno[2',3':4,5]pyrrolo[1,2-d][1,4]benzodiazepine-10-carboxylate

There total 2 articles about methyl 12-cyclohexyl-6-oxo-6,7-dihydro-5H-thieno[2',3':4,5]pyrrolo[1,2-d][1,4]benzodiazepine-10-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 886973-25-7
methyl 5-[2-(2-chloroacetylamino)phenyl]-6-cyclohexyl-4H-thieno[3,2-b]pyrrole-2-carboxylate

: 886972-70-9
methyl 12-cyclohexyl-6-oxo-6,7-dihydro-5H-thieno[2',3':4,5]pyrrolo[1,2-d][1,4]benzodiazepine-10-carboxylate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 1h;

Reference yield:

: 914498-00-3
methyl 5-{2-[(tert-butoxy-carbonyl)amino]phenyl}-4-(2-tert-butoxy-2-oxoethyl)-6-cyclohexyl-4H-thieno[3,2-b]pyrrole-2-carboxylate

: 886972-70-9
methyl 12-cyclohexyl-6-oxo-6,7-dihydro-5H-thieno[2',3':4,5]pyrrolo[1,2-d][1,4]benzodiazepine-10-carboxylate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 - 40 ℃; for 2.5h;

Reference yield: 100.0%

: 886972-70-9
methyl 12-cyclohexyl-6-oxo-6,7-dihydro-5H-thieno[2',3':4,5]pyrrolo[1,2-d][1,4]benzodiazepine-10-carboxylate

: methyl 11-cyclohexyl-5,6-dihydro-4H-1-thia-3b,6-diazabenzo[e]cyclopenta[a]azulene-2-carboxylate

Guidance literature:: methyl 12-cyclohexyl-6-oxo-6,7-dihydro-5H-thieno[2',3':4,5]pyrrolo[1,2-d][1,4]benzodiazepine-10-carboxylate; With borane-THF; In tetrahydrofuran; at 0 - 20 ℃; for 14h;

With hydrogenchloride; In tetrahydrofuran; water; at 70 ℃; for 2h;

With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃;