N-[(2S,3S,4R)-3,4-dihydroxy-1-(trityloxy)octadecan-2-yl]-2,2,2-trifluoroacetamide

Base Information

Chemical Name:N-[(2S,3S,4R)-3,4-dihydroxy-1-(trityloxy)octadecan-2-yl]-2,2,2-trifluoroacetamide
CAS No.:1310058-04-8
Molecular Formula:C₃₉H₅₂F₃NO₄
Molecular Weight:655.841
Hs Code.:

Synonyms:N-[(2S,3S,4R)-3,4-dihydroxy-1-(trityloxy)octadecan-2-yl]-2,2,2-trifluoroacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(2S,3S,4R)-3,4-dihydroxy-1-(trityloxy)octadecan-2-yl]-2,2,2-trifluoroacetamide

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Technology Process of N-[(2S,3S,4R)-3,4-dihydroxy-1-(trityloxy)octadecan-2-yl]-2,2,2-trifluoroacetamide

There total 1 articles about N-[(2S,3S,4R)-3,4-dihydroxy-1-(trityloxy)octadecan-2-yl]-2,2,2-trifluoroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 76-83-5
trityl chloride

: 354149-81-8
2,2,2-trifluoro-N-[(2S,3S,4R)-1,3,4-trihydroxyoctadecan-2-yl]acetamide

: 1310058-04-8
N-[(2S,3S,4R)-3,4-dihydroxy-1-(trityloxy)octadecan-2-yl]-2,2,2-trifluoroacetamide

Guidance literature:: With pyridine; dmap; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1055/s-0030-1258437

Reference yield:

: 1310058-04-8
N-[(2S,3S,4R)-3,4-dihydroxy-1-(trityloxy)octadecan-2-yl]-2,2,2-trifluoroacetamide

: C₃₉H₅₀F₃NO₅S

Guidance literature:: With thionyl chloride; triethylamine; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1055/s-0030-1258437

Reference yield:

: 1310058-04-8
N-[(2S,3S,4R)-3,4-dihydroxy-1-(trityloxy)octadecan-2-yl]-2,2,2-trifluoroacetamide

: (2S,3S,4S)-1-(trityloxy)-2-[N-(trifluoroacetyl)amino]octadecan-3,4-cyclic sulfate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2: sodium periodate; ruthenium(III) chloride trihydrate / tetrachloromethane; water; acetonitrile / 2 h / 20 °C / Inert atmosphere

With sodium periodate; thionyl chloride; ruthenium(III) chloride trihydrate; triethylamine; In tetrachloromethane; dichloromethane; water; acetonitrile;
DOI:10.1055/s-0030-1258437