2-{[1-(trans-4-methylcyclohexyl)-1H-imidazol-4-yl]methyl}morpholin-3-one

Base Information

Chemical Name:2-{[1-(trans-4-methylcyclohexyl)-1H-imidazol-4-yl]methyl}morpholin-3-one
CAS No.:1335139-80-4
Molecular Formula:C₁₅H₂₃N₃O₂
Molecular Weight:277.367
Hs Code.:

Synonyms:2-{[1-(trans-4-methylcyclohexyl)-1H-imidazol-4-yl]methyl}morpholin-3-one

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Chemical Property of 2-{[1-(trans-4-methylcyclohexyl)-1H-imidazol-4-yl]methyl}morpholin-3-one

Chemical Property:

Purity/Quality:

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Technology Process of 2-{[1-(trans-4-methylcyclohexyl)-1H-imidazol-4-yl]methyl}morpholin-3-one

There total 5 articles about 2-{[1-(trans-4-methylcyclohexyl)-1H-imidazol-4-yl]methyl}morpholin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1335139-79-1
(2Z)-2-{[1-(trans-4-methylcyclohexyl)-1H-imidazol-4-yl]methylene}morpholin-3-one

: 1335139-80-4
2-{[1-(trans-4-methylcyclohexyl)-1H-imidazol-4-yl]methyl}morpholin-3-one

Guidance literature:: With palladium 10% on activated carbon; water; hydrogen; In ethanol; at 20 - 45 ℃; for 2h; under 760.051 Torr;

Reference yield:

: 1335139-08-6
1-(trans-4-methylcyclohexyl)-1H-imidazole-4-carbaldehyde

: 1335139-80-4
2-{[1-(trans-4-methylcyclohexyl)-1H-imidazol-4-yl]methyl}morpholin-3-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran; hexane / 0.5 h / -78 °C

1.2: 15 h / -78 - 20 °C

2.1: palladium 10% on activated carbon; hydrogen; water / ethanol / 2 h / 20 - 45 °C / 760.05 Torr

With palladium 10% on activated carbon; water; hydrogen; lithium hexamethyldisilazane; In tetrahydrofuran; ethanol; hexane;

Reference yield:

: 2523-55-9
trans-4-methylcyclohexanamine

: 1335139-80-4
2-{[1-(trans-4-methylcyclohexyl)-1H-imidazol-4-yl]methyl}morpholin-3-one

Guidance literature:: Multi-step reaction with 5 steps

1.1: 4 h / 70 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

3.1: sodium hydrogencarbonate; iodine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / water; toluene / 2 h / 20 °C

4.1: lithium hexamethyldisilazane / tetrahydrofuran; hexane / 0.5 h / -78 °C

4.2: 15 h / -78 - 20 °C

5.1: palladium 10% on activated carbon; hydrogen; water / ethanol / 2 h / 20 - 45 °C / 760.05 Torr

With lithium aluminium tetrahydride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; palladium 10% on activated carbon; water; hydrogen; iodine; sodium hydrogencarbonate; lithium hexamethyldisilazane; In tetrahydrofuran; ethanol; hexane; water; toluene;