1-<<3--3-methylbutoxy>methyl>-4-methoxybenzene

Base Information

Chemical Name:1-<<3--3-methylbutoxy>methyl>-4-methoxybenzene
CAS No.:170474-54-1
Molecular Formula:C₁₇H₂₆O₂Si
Molecular Weight:290.478
Hs Code.:

1-<<3-<ethynyl(dimethyl)silyl>-3-methylbutoxy>methyl>-4-methoxybenzene

Synonyms:1-<<3--3-methylbutoxy>methyl>-4-methoxybenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<<3--3-methylbutoxy>methyl>-4-methoxybenzene

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Technology Process of 1-<<3--3-methylbutoxy>methyl>-4-methoxybenzene

There total 1 articles about 1-<<3--3-methylbutoxy>methyl>-4-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 170474-47-2
1-<<3-silyl>-3-methylbutoxy>methyl>-4-methoxybenzene

: 170474-54-1
1-<<3--3-methylbutoxy>methyl>-4-methoxybenzene

Guidance literature:: With potassium carbonate; In methanol; Ambient temperature;
DOI:10.1002/hlca.19950780319

Reference yield:

: 13096-62-3
(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-one

: 170474-54-1
1-<<3--3-methylbutoxy>methyl>-4-methoxybenzene

: 4,5,6,8-tetra-O-benzyl-1,1,2,2-tetradehydro-1,2-dideoxy-1-C-<<1,1-dimethyl-3-(4-methoxybenzyloxy)propyl>dimethylsilyl>-α-D-gluco-oct-3-ulopyranose

: 4,5,6,8-tetra-O-benzyl-1,1,2,2-tetradehydro-1,2-dideoxy-1-C-<<1,1-dimethyl-3-(4-methoxybenzyloxy)propyl>dimethylsilyl>-β-D-gluco-oct-3-ulopyranose

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; Yield given. Yields of byproduct given. Title compound not separated from byproducts; -76 degC, 45 min, -76 degC to r. t. within 10 min;
DOI:10.1002/hlca.19950780319

Reference yield:

: 170474-54-1
1-<<3--3-methylbutoxy>methyl>-4-methoxybenzene

: 167646-36-8
2,3,6-tri-O-benzyl-4-deoxy-4-C-(2,2-dibromoethenyl)-D-glucono-1,5-lactone

: 4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-6-C-(2,2-dibromoethenyl)-1-C-<<1,1-dimethyl-3-(4-methoxybenzyloxy)propyl>dimethylsilyl>-α-D-gluco-oct-3-ulopyranose

: 4,5,8-tri-O-benzyl-1,1,2,2-tetradehydro-1,2,6-trideoxy-6-C-(2,2-dibromoethenyl)-1-C-<<1,1-dimethyl-3-(4-methoxybenzyloxy)propyl>dimethylsilyl>-β-D-gluco-oct-3-ulopyranose

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) THF, hexane, -76 degC, 20 min, -76 to -15 degC, 10 min, -15 degC, 10 min; 2.) -76 degC, 0.5 h;
DOI:10.1002/hlca.19950780319