heptabutylphosphorimidic triamide

Base Information

• Chemical Name: heptabutylphosphorimidic triamide
• CAS No.: 80166-33-2
• Molecular Formula: C₂₈H₆₃N₄P
• Molecular Weight: 486.809

Synonyms:heptabutylphosphorimidic triamide

Chemical Property of heptabutylphosphorimidic triamide

Chemical Property:

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Technology Process of heptabutylphosphorimidic triamide

There total 2 articles about heptabutylphosphorimidic triamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

tetrakis(dibutylamino)phosphonium bromide → N-pentylidenehexan-1-amine (10599-77-6) + heptabutylphosphorimidic triamide (80166-33-2) + N-butylamine (109-73-9,85404-21-3) + hexabutyl triamidophosphite (5848-65-7)

Guidance literature:

With sodium amide; at 180 ℃; under 0.02 Torr; Product distribution; Mechanism;

Reference yield:

tetrakis(dibutylamino)phosphonium hexafluorophosphate → hexabutylphosphoric acid triamide (22421-85-8) + heptabutylphosphorimidic triamide (80166-33-2)

Guidance literature:

With potassium hydroxide; at 160 ℃; for 4h; Sealed tube; Inert atmosphere;

DOI:10.1021/acs.organomet.7b00663

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