tetraphenylarsonium oxo(N,N'-propylenebis(2-mercaptoacetimido))technetate

Base Information

Chemical Name:tetraphenylarsonium oxo(N,N'-propylenebis(2-mercaptoacetimido))technetate
CAS No.:75949-48-3
Molecular Formula:C₇H₁₀N₂O₃S₂Tc*C₂₄H₂₀As
Molecular Weight:715.552
Hs Code.:

Synonyms:tetraphenylarsonium oxo(N,N'-propylenebis(2-mercaptoacetimido))technetate

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Chemical Property of tetraphenylarsonium oxo(N,N'-propylenebis(2-mercaptoacetimido))technetate

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Technology Process of tetraphenylarsonium oxo(N,N'-propylenebis(2-mercaptoacetimido))technetate

There total 1 articles about tetraphenylarsonium oxo(N,N'-propylenebis(2-mercaptoacetimido))technetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 34035-97-7
ammonium pertechnetate

: 104170-16-3
tetraphenylarsonium chloride monohydrate

: 75948-93-5
N,N'-propylenebis(benzoyl-2-mercaptoacetamide)

: 75949-48-3
tetraphenylarsonium oxo(N,N'-propylenebis(2-mercaptoacetimido))technetate

Guidance literature:: With sodium hydroxide; sodium dithionite; In ethanol; water; suspn. 3-fold excess pbma in mixt. water-ethanol heated to 70°C to dissolve ligand, pH adjusted to 13 with NaOH, NH4TcO4 soln. added, sodium dithionite in water added, soln. cooled, Ph4AsCl added; after standing for 12 h, solid separated and recrystd. from ethanol/water by slow evapn.; elem. anal.;
DOI:10.1021/ic50220a001