cyclo--5-methylheptanoyl>oxy-3-oxo-2,5-dimethylhexanoyl>-L-leucyl>-L-prolyl-N,O-dimethyl-L-tyrosyl>-L-threonyl> hydrochloride

Base Information

• Chemical Name: cyclo--5-methylheptanoyl>oxy-3-oxo-2,5-dimethylhexanoyl>-L-leucyl>-L-prolyl-N,O-dimethyl-L-tyrosyl>-L-threonyl> hydrochloride
• CAS No.: 130008-93-4
• Molecular Formula: C₄₂H₆₅N₅O₁₁*ClH
• Molecular Weight: 852.466

Synonyms:cyclo--5-methylheptanoyl>oxy-3-oxo-2,5-dimethylhexanoyl>-L-leucyl>-L-prolyl-N,O-dimethyl-L-tyrosyl>-L-threonyl> hydrochloride

Chemical Property of cyclo--5-methylheptanoyl>oxy-3-oxo-2,5-dimethylhexanoyl>-L-leucyl>-L-prolyl-N,O-dimethyl-L-tyrosyl>-L-threonyl> hydrochloride

Chemical Property:

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Technology Process of cyclo--5-methylheptanoyl>oxy-3-oxo-2,5-dimethylhexanoyl>-L-leucyl>-L-prolyl-N,O-dimethyl-L-tyrosyl>-L-threonyl> hydrochloride

There total 24 articles about cyclo--5-methylheptanoyl>oxy-3-oxo-2,5-dimethylhexanoyl>-L-leucyl>-L-prolyl-N,O-dimethyl-L-tyrosyl>-L-threonyl> hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C50H71N5O13 (118878-64-1) → cyclo--5-methylheptanoyl>oxy-3-oxo-2,5-dimethylhexanoyl>-L-leucyl>-L-prolyl-N,O-dimethyl-L-tyrosyl>-L-threonyl> hydrochloride (130008-93-4)

Guidance literature:

With hydrogenchloride; hydrogen; palladium on activated charcoal; In acetic acid; for 3h; under 2280 Torr;

DOI:10.1055/s-1991-26448

Reference yield: 90.0%

cyclo--5-methylheptanoyl>oxy-3-oxo-2,5-dimethylhexanoyl>-L-leucyl>-L-prolyl-N,O-dimethyl-L-tyrosyl>-L-threonyl> (129942-52-5) → cyclo--5-methylheptanoyl>oxy-3-oxo-2,5-dimethylhexanoyl>-L-leucyl>-L-prolyl-N,O-dimethyl-L-tyrosyl>-L-threonyl> hydrochloride (130008-93-4)

Guidance literature:

With hydrogenchloride; In ethyl acetate; 1.) from -20 deg C to -10 deg C, 2 h, 2.) 0 deg C, 4 h;

DOI:10.1021/ja00177a030

Reference yield: 90.0%

C56H93N5O13Si (129942-52-5) → (5S,8S,10S,14S,15R,18S,19R,22S,24aS)-18-Amino-15-((R)-sec-butyl)-14-hydroxy-5-isobutyl-10-isopropyl-22-(4-methoxy-benzyl)-8,19,23-trimethyl-tetradecahydro-11,20-dioxa-3a,6,16,23-tetraaza-cyclopentacyclotricosene-4,7,9,12,17,21,24-heptaone; hydrochloride (130008-93-4)

Guidance literature:

With hydrogenchloride; In ethyl acetate; at -30 - 0 ℃;

DOI:10.1016/S0040-4039(01)80647-X

upstream raw materials:

cyclo--5-methylheptanoyl>oxy-3-oxo-2,5-dimethylhexanoyl>-L-leucyl>-L-prolyl-N,O-dimethyl-L-tyrosyl>-L-threonyl>

C₅₀H₇₁N₅O₁₃

cyclo--5-methylheptanoyl>oxy-3-hydroxy-2,5-dimethylhexanoyl>-L-leucyl>-L-prolyl-N,O-dimethyl-L-tyrosyl>-L-threonyl>

1-(tert-butoxycarbonyl)-L-proline

Downstream raw materials:

N-Z-didemnin A

didemnin B

C₅₉H₉₁N₇O₁₅

C₆₂H₈₉N₇O₁₅

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