N-[1-(1H-benzotriazol-1-yl)-2-(N-methylanilino)ethylidene]-2,5-dichloroaniline

Base Information

• Chemical Name: N-[1-(1H-benzotriazol-1-yl)-2-(N-methylanilino)ethylidene]-2,5-dichloroaniline
• CAS No.: 342632-62-6
• Molecular Formula: C₂₁H₁₇Cl₂N₅
• Molecular Weight: 410.305
• Mol file: 342632-62-6.mol

Synonyms:N-[1-(1H-benzotriazol-1-yl)-2-(N-methylanilino)ethylidene]-2,5-dichloroaniline

Chemical Property of N-[1-(1H-benzotriazol-1-yl)-2-(N-methylanilino)ethylidene]-2,5-dichloroaniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of N-[1-(1H-benzotriazol-1-yl)-2-(N-methylanilino)ethylidene]-2,5-dichloroaniline

There total 1 articles about N-[1-(1H-benzotriazol-1-yl)-2-(N-methylanilino)ethylidene]-2,5-dichloroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

N-((1H-benzo(d)(1,2,3)triazol-1-yl)methyl)-N-methylaniline (15497-51-5) + 1-isocyano-2,5-dichlorobenzene (245539-10-0) → N-[1-(1H-benzotriazol-1-yl)-2-(N-methylanilino)ethylidene]-2,5-dichloroaniline (342632-62-6)

Guidance literature:

With boron trifluoride diethyl etherate; In tetrahydrofuran; at 25 ℃;

DOI:10.1021/jo0016935

Reference yield: 92.0%

thiophenol (108-98-5) + N-[1-(1H-benzotriazol-1-yl)-2-(N-methylanilino)ethylidene]-2,5-dichloroaniline (342632-62-6) → phenyl N'-(2,5-dichlorophenyl)-2-(N-methyl-N-phenylamino)thioacetimidate

Guidance literature:

With sodium methylate; In tetrahydrofuran; for 18h; Heating;

DOI:10.1021/jo0016935

Reference yield: 32.0%

N-[1-(1H-benzotriazol-1-yl)-2-(N-methylanilino)ethylidene]-2,5-dichloroaniline (342632-62-6) → N-(2,5-dichlorophenyl)-2-(N-methylanilino)acetamide + N'-(2,5-dichlorophenyl)-N-methyl-2-(N-methylanilino)-N-phenylethanimidamide

Guidance literature:

With silica gel; In hexane; ethyl acetate;

DOI:10.1021/jo0016935

upstream raw materials:

N-((1H-benzo(d)(1,2,3)triazol-1-yl)methyl)-N-methylaniline

1-isocyano-2,5-dichlorobenzene