tert-butyl-[5-(2,2-dibromo-1-fluoro-vinyl)-2-methoxy-phenoxy]-dimethyl-silane

Base Information

• Chemical Name: tert-butyl-[5-(2,2-dibromo-1-fluoro-vinyl)-2-methoxy-phenoxy]-dimethyl-silane
• CAS No.: 1021916-49-3
• Molecular Formula: C₁₅H₂₁Br₂FO₂Si
• Molecular Weight: 440.222

Synonyms:tert-butyl-[5-(2,2-dibromo-1-fluoro-vinyl)-2-methoxy-phenoxy]-dimethyl-silane

Chemical Property of tert-butyl-[5-(2,2-dibromo-1-fluoro-vinyl)-2-methoxy-phenoxy]-dimethyl-silane

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Technology Process of tert-butyl-[5-(2,2-dibromo-1-fluoro-vinyl)-2-methoxy-phenoxy]-dimethyl-silane

There total 1 articles about tert-butyl-[5-(2,2-dibromo-1-fluoro-vinyl)-2-methoxy-phenoxy]-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

tert-butyl-[2-methoxy-5-(2,2,2-tribromo-1-fluoro-ethyl)-phenoxy]-dimethyl-silane (1021916-47-1) → tert-butyl-[5-(2,2-dibromo-1-fluoro-vinyl)-2-methoxy-phenoxy]-dimethyl-silane (1021916-49-3)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃;

DOI:10.1021/jm701362m

Reference yield: 89.0%

tert-butyl-[5-(2,2-dibromo-1-fluoro-vinyl)-2-methoxy-phenoxy]-dimethyl-silane (1021916-49-3) → C15H22BrFO2Si

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In 1,2-dichloro-ethane; Heating;

DOI:10.1021/jm701362m

Reference yield: 32.0%

tert-butyl-[5-(2,2-dibromo-1-fluoro-vinyl)-2-methoxy-phenoxy]-dimethyl-silane (1021916-49-3) + 3,4,5-trimethoxyphenylboronic Acid (182163-96-8) → {5-[(Z)-2-bromo-1-fluoro-2-(3,4,5-trimethoxy-phenyl)-vinyl]-2-methoxy-phenoxy}-tert-butyl-dimethyl-silane (1021916-78-8) + {5-[(E)-2-bromo-1-fluoro-2-(3,4,5-trimethoxy-phenyl)-vinyl]-2-methoxy-phenoxy}-tert-butyl-dimethyl-silane (1021916-51-7)

Guidance literature:

With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; Heating;

DOI:10.1021/jm701362m

upstream raw materials:

tert-butyl-[2-methoxy-5-(2,2,2-tribromo-1-fluoro-ethyl)-phenoxy]-dimethyl-silane

Downstream raw materials:

{5-[(Z)-2-bromo-1-fluoro-2-(3,4,5-trimethoxy-phenyl)-vinyl]-2-methoxy-phenoxy}-tert-butyl-dimethyl-silane

{5-[(E)-2-bromo-1-fluoro-2-(3,4,5-trimethoxy-phenyl)-vinyl]-2-methoxy-phenoxy}-tert-butyl-dimethyl-silane

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