N-[4-[(3-bromophenyl)-amino]-quinazolin-6-yl]-3-morpholino-propylamide

Base Information

• Chemical Name: N-[4-[(3-bromophenyl)-amino]-quinazolin-6-yl]-3-morpholino-propylamide
• CAS No.: 198961-88-5
• Molecular Formula: C₂₁H₂₂BrN₅O₂
• Molecular Weight: 456.342

Synonyms:N-[4-[(3-bromophenyl)-amino]-quinazolin-6-yl]-3-morpholino-propylamide

Chemical Property of N-[4-[(3-bromophenyl)-amino]-quinazolin-6-yl]-3-morpholino-propylamide

Chemical Property:

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Technology Process of N-[4-[(3-bromophenyl)-amino]-quinazolin-6-yl]-3-morpholino-propylamide

There total 7 articles about N-[4-[(3-bromophenyl)-amino]-quinazolin-6-yl]-3-morpholino-propylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

morpholine (110-91-8,99108-56-2) + PD 168393 (194423-15-9) → N-[4-[(3-bromophenyl)-amino]-quinazolin-6-yl]-3-morpholino-propylamide (198961-88-5)

Guidance literature:

With toluene-4-sulfonic acid; In tetrahydrofuran; at 50 ℃; for 4h;

DOI:10.1021/jm000372i

Reference yield: 70.0%

morpholine (110-91-8,99108-56-2) + N-(4-((3-bromophenyl)amino)quinazolin-6-yl)-3-chloropropanamide (1233953-80-4) → N-[4-[(3-bromophenyl)-amino]-quinazolin-6-yl]-3-morpholino-propylamide (198961-88-5)

Guidance literature:

morpholine; N-(4-((3-bromophenyl)amino)quinazolin-6-yl)-3-chloropropanamide; With potassium iodide; In ethanol; Reflux;

With potassium hydroxide; In ethanol; at 0 ℃;

DOI:10.1021/jm201507x

Reference yield: 70.0%

→ N-[4-[(3-bromophenyl)-amino]-quinazolin-6-yl]-3-morpholino-propylamide (198961-88-5)

Guidance literature:

upstream raw materials:

morpholine

PD 168393

N-(4-((3-bromophenyl)amino)quinazolin-6-yl)-3-chloropropanamide

5-nitroanthranilonitrile

Downstream raw materials:

N⁴-(3-bromophenyl)-N⁶-[3-(4-morpholinyl)propyl]-4,6-quinazolinediamine

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