1-allyl-1H-indole-2-carboxylic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester

Base Information

Chemical Name:1-allyl-1H-indole-2-carboxylic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester
CAS No.:794588-64-0
Molecular Formula:C₂₈H₃₃NO₅
Molecular Weight:463.574
Hs Code.:

Synonyms:1-allyl-1H-indole-2-carboxylic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-allyl-1H-indole-2-carboxylic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester

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Technology Process of 1-allyl-1H-indole-2-carboxylic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester

There total 2 articles about 1-allyl-1H-indole-2-carboxylic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 155193-48-9
1-Allyl-1H-indole-2-carboxylic acid

: 794588-45-7
1-allyloxy-5-(4-methoxybenzyloxy)pentan-3-ol

: 794588-64-0
1-allyl-1H-indole-2-carboxylic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In diethyl ether; at 0 - 20 ℃;
DOI:10.1016/j.tet.2004.06.146

Reference yield:

: 794588-83-3
(S)-3-(tert-butyldimethylsilyloxy)-5-(4-methoxybenzyloxy)pentan-1-ol

: 794588-64-0
1-allyl-1H-indole-2-carboxylic acid 1-(2-allyloxyethyl)-3-(4-methoxybenzyloxy)propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / NaH / tetrahydrofuran / 20 h / 20 °C

2: 74 percent / TBAF / tetrahydrofuran / 5 h / 20 °C

3: 100 percent / diisopropyl azodicarboxylate; PPh₃ / diethyl ether / 0 - 20 °C

With di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; sodium hydride; triphenylphosphine; In tetrahydrofuran; diethyl ether; 3: Mitsunobu reaction;
DOI:10.1016/j.tet.2004.06.146