(2,4,6-trimethylbenzene-1,3,5-triyl)tris(methylene) tris(2,3,4,5-tetrafluoro-6-iodobenzoate)

Base Information

• Chemical Name: (2,4,6-trimethylbenzene-1,3,5-triyl)tris(methylene) tris(2,3,4,5-tetrafluoro-6-iodobenzoate)
• CAS No.: 1221690-64-7
• Molecular Formula: C₃₃H₁₅F₁₂I₃O₆
• Molecular Weight: 1116.17

Synonyms:(2,4,6-trimethylbenzene-1,3,5-triyl)tris(methylene) tris(2,3,4,5-tetrafluoro-6-iodobenzoate)

Chemical Property of (2,4,6-trimethylbenzene-1,3,5-triyl)tris(methylene) tris(2,3,4,5-tetrafluoro-6-iodobenzoate)

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Technology Process of (2,4,6-trimethylbenzene-1,3,5-triyl)tris(methylene) tris(2,3,4,5-tetrafluoro-6-iodobenzoate)

There total 1 articles about (2,4,6-trimethylbenzene-1,3,5-triyl)tris(methylene) tris(2,3,4,5-tetrafluoro-6-iodobenzoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

1,3,5-tris(bromomethyl)-2,4,6-trimethylbenzene (21988-87-4) + 2,3,4,5-tetrafluoro-6-iodobenzoic acid (110625-15-5) → (2,4,6-trimethylbenzene-1,3,5-triyl)tris(methylene) tris(2,3,4,5-tetrafluoro-6-iodobenzoate) (1221690-64-7)

Guidance literature:

2,3,4,5-tetrafluoro-6-iodobenzoic acid; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; for 0.25h; Inert atmosphere;

1,3,5-tris(bromomethyl)-2,4,6-trimethylbenzene; In acetonitrile; at 25 ℃; for 6h; Inert atmosphere;

DOI:10.1002/anie.200906488

Reference yield:

(2,4,6-trimethylbenzene-1,3,5-triyl)tris(methylene) tris(2,3,4,5-tetrafluoro-6-iodobenzoate) (1221690-64-7) + tetrabutyl-ammonium chloride (1112-67-0) → C16H36N(1+)*C33H15F12I3O6*Cl(1-)

Guidance literature:

In acetone; at 21.84 ℃;

DOI:10.1002/anie.200906488

Reference yield:

(2,4,6-trimethylbenzene-1,3,5-triyl)tris(methylene) tris(2,3,4,5-tetrafluoro-6-iodobenzoate) (1221690-64-7) + tetrabutylammomium bromide (1643-19-2) → Br(1-)*C16H36N(1+)*C33H15F12I3O6

Guidance literature:

In acetone; at 21.84 ℃;

DOI:10.1002/anie.200906488

upstream raw materials:

1,3,5-tris(bromomethyl)-2,4,6-trimethylbenzene

2,3,4,5-tetrafluoro-6-iodobenzoic acid

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