carbonyl(η5-cyclopentadienyl)(α-4-methylphenylacetic acid)(trifluorophosphine)(trimethylphosphine)tungsten

Base Information

• Chemical Name: carbonyl(η5-cyclopentadienyl)(α-4-methylphenylacetic acid)(trifluorophosphine)(trimethylphosphine)tungsten
• CAS No.: 84577-19-5
• Molecular Formula: C₁₈H₂₃F₃O₃P₂W
• Molecular Weight: 590.172

Synonyms:carbonyl(η5-cyclopentadienyl)(α-4-methylphenylacetic acid)(trifluorophosphine)(trimethylphosphine)tungsten

Chemical Property of carbonyl(η5-cyclopentadienyl)(α-4-methylphenylacetic acid)(trifluorophosphine)(trimethylphosphine)tungsten

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Technology Process of carbonyl(η5-cyclopentadienyl)(α-4-methylphenylacetic acid)(trifluorophosphine)(trimethylphosphine)tungsten

There total 1 articles about carbonyl(η5-cyclopentadienyl)(α-4-methylphenylacetic acid)(trifluorophosphine)(trimethylphosphine)tungsten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

carbonyl(η5-cyclopentadienyl)(η2-4-methylphenylketenyl)trimethylphosphinetungsten → carbonyl(η5-cyclopentadienyl)(α-4-methylphenylacetic acid)(trifluorophosphine)(trimethylphosphine)tungsten (84577-19-5)

Guidance literature:

With water; trifluorophosphane; In diethyl ether; dichloromethane; educt soln. in CH2Cl2; -78°C, dry PF3 stream; -78°C, 3.5 M HCl in ether, Ar-satd. water; stirring for 3 h; pptn. with ether/pentane, chromy. (SiO2, CH2Cl2/ether, -30°C), drying in high vac. (-20°C, 8 h); elem. anal.;

DOI:10.1016/S0022-328X(00)87072-2

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