tert-butyl 4-(9H-benzo[f]pyrido[2,3-b][1,2,4]triazolo[4,3-d][1,4]diazepin-3-yl)phenethylcarbamate

Base Information

Chemical Name:tert-butyl 4-(9H-benzo[f]pyrido[2,3-b][1,2,4]triazolo[4,3-d][1,4]diazepin-3-yl)phenethylcarbamate
CAS No.:1338243-49-4
Molecular Formula:C₂₆H₂₆N₆O₂
Molecular Weight:454.531
Hs Code.:

Synonyms:tert-butyl 4-(9H-benzo[f]pyrido[2,3-b][1,2,4]triazolo[4,3-d][1,4]diazepin-3-yl)phenethylcarbamate

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Chemical Property of tert-butyl 4-(9H-benzo[f]pyrido[2,3-b][1,2,4]triazolo[4,3-d][1,4]diazepin-3-yl)phenethylcarbamate

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Technology Process of tert-butyl 4-(9H-benzo[f]pyrido[2,3-b][1,2,4]triazolo[4,3-d][1,4]diazepin-3-yl)phenethylcarbamate

There total 3 articles about tert-butyl 4-(9H-benzo[f]pyrido[2,3-b][1,2,4]triazolo[4,3-d][1,4]diazepin-3-yl)phenethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1338243-73-4
6-chloro-11H-benzo[e]pyrido[3,2-b][1,4]diazepine

: 1338243-75-6
tert-butyl 4-(hydrazinecarbonyl)phenethylcarbamate

: 1338243-49-4
tert-butyl 4-(9H-benzo[f]pyrido[2,3-b][1,2,4]triazolo[4,3-d][1,4]diazepin-3-yl)phenethylcarbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl acetamide; at 80 - 100 ℃; for 72h;

Reference yield:

: 132690-91-6
4-[2-(tert-butyloxycarbonylamino)ethyl]benzoic acid

: 1338243-49-4
tert-butyl 4-(9H-benzo[f]pyrido[2,3-b][1,2,4]triazolo[4,3-d][1,4]diazepin-3-yl)phenethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,1'-carbonyldiimidazole / dichloromethane / 0.75 h / 20 °C

1.2: 16 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl acetamide / 72 h / 80 - 100 °C

With N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole; In dichloromethane; N,N-dimethyl acetamide;

Reference yield:

: 885-70-1
5H-benzo[e]pyrido[3,2-b][1,4]diazepin-6(11H)-one

: 1338243-49-4
tert-butyl 4-(9H-benzo[f]pyrido[2,3-b][1,2,4]triazolo[4,3-d][1,4]diazepin-3-yl)phenethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus pentachloride / dichloromethane / Reflux

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl acetamide / 72 h / 80 - 100 °C

With phosphorus pentachloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl acetamide;