Carbamic acid, [(1R,3E)-1-(hydroxymethyl)-3-pentenyl]-, 1,1-dimethylethyl

Base Information

Chemical Name:Carbamic acid, [(1R,3E)-1-(hydroxymethyl)-3-pentenyl]-, 1,1-dimethylethyl
CAS No.:334994-39-7
Molecular Formula:C₁₁H₂₁NO₃
Molecular Weight:215.293
Hs Code.:
Mol file:334994-39-7.mol

Synonyms:Carbamic acid, [(1R,3E)-1-(hydroxymethyl)-3-pentenyl]-, 1,1-dimethylethyl

Suppliers and Price of Carbamic acid, [(1R,3E)-1-(hydroxymethyl)-3-pentenyl]-, 1,1-dimethylethyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Carbamic acid, [(1R,3E)-1-(hydroxymethyl)-3-pentenyl]-, 1,1-dimethylethyl

Chemical Property:

PSA：58.56000
LogP:2.22910

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, [(1R,3E)-1-(hydroxymethyl)-3-pentenyl]-, 1,1-dimethylethyl

There total 3 articles about Carbamic acid, [(1R,3E)-1-(hydroxymethyl)-3-pentenyl]-, 1,1-dimethylethyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 334994-38-6
2-(R)-tert-butoxycarbonylamino-hex-4-(E)-enoic acid

: 334994-40-0
2-(R,E)-aminohex-4-en-1-ol

: 335386-73-7
((E)-(R)-1-Formyl-pent-3-enyl)-carbamic acid tert-butyl ester

: 334994-39-7
((E)-(R)-1-Hydroxymethyl-pent-3-enyl)-carbamic acid tert-butyl ester

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/S0040-4039(00)01921-3

Reference yield:

: 112741-49-8,173397-90-5
tert-butyl (2R,3S)-6-oxo-2,3-diphenylmorpholine-4-carboxylate

: 334994-39-7
((E)-(R)-1-Hydroxymethyl-pent-3-enyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / sodium bis(hexamethylsilyl)amide / tetrahydrofuran

2: 57 percent / Li / liquid ammonia

3: lithium aluminum hydride / tetrahydrofuran / 0 °C

With lithium aluminium tetrahydride; sodium hexamethyldisilazane; lithium; In tetrahydrofuran; ammonia; 2: Birch reduction;
DOI:10.1016/S0040-4039(00)01921-3

Reference yield:

: 334994-43-3
(3S,5S,6R)-3-((E)-But-2-enyl)-2-oxo-5,6-diphenyl-morpholine-4-carboxylic acid tert-butyl ester

: 334994-39-7
((E)-(R)-1-Hydroxymethyl-pent-3-enyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / Li / liquid ammonia

2: lithium aluminum hydride / tetrahydrofuran / 0 °C

With lithium aluminium tetrahydride; lithium; In tetrahydrofuran; ammonia; 1: Birch reduction;
DOI:10.1016/S0040-4039(00)01921-3