Technology Process of C34H32NOP
There total 8 articles about C34H32NOP which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dmap;
In
diethyl ether;
at 20 ℃;
for 0.5h;
DOI:10.1039/b313979d
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: n-BuLi / 1 h / -50 °C
1.2: CuCN*2LiCl / -80 °C
1.3: 40 percent / TMSCl / -80 °C
2.1: 80 percent / -80 - 20 °C
3.1: 80 percent / Alpine-Borane / 0 - 20 °C
4.1: 70 percent / Bu3SnH / PdCl2(PPh3)2 / tetrahydrofuran / 0.5 h / 20 °C
5.1: 80 percent / I2 / CH2Cl2 / 20 °C
6.1: 25 percent / tetrahydrofuran / 48 h / 65 °C
7.1: 95 percent / DMAP / diethyl ether / 0.5 h / 20 °C
With
dmap; n-butyllithium; Alpine borane; iodine; tri-n-butyl-tin hydride;
bis-triphenylphosphine-palladium(II) chloride;
In
tetrahydrofuran; diethyl ether; dichloromethane;
3.1: Swern oxidation;
DOI:10.1039/b313979d
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 80 percent / -80 - 20 °C
2: 80 percent / Alpine-Borane / 0 - 20 °C
3: 70 percent / Bu3SnH / PdCl2(PPh3)2 / tetrahydrofuran / 0.5 h / 20 °C
4: 80 percent / I2 / CH2Cl2 / 20 °C
5: 25 percent / tetrahydrofuran / 48 h / 65 °C
6: 95 percent / DMAP / diethyl ether / 0.5 h / 20 °C
With
dmap; Alpine borane; iodine; tri-n-butyl-tin hydride;
bis-triphenylphosphine-palladium(II) chloride;
In
tetrahydrofuran; diethyl ether; dichloromethane;
2: Swern oxidation;
DOI:10.1039/b313979d
