N^α-(benzyloxycarbonyl)tryptophanyl-N^ε-(benzyloxycarbonyl)lysine methyl ester

Base Information

Chemical Name:N^α-(benzyloxycarbonyl)tryptophanyl-N^ε-(benzyloxycarbonyl)lysine methyl ester
CAS No.:111237-83-3
Molecular Formula:C₃₄H₃₈N₄O₇
Molecular Weight:614.698
Hs Code.:

N<sup>α</sup>-(benzyloxycarbonyl)tryptophanyl-N<sup>ε</sup>-(benzyloxycarbonyl)lysine methyl ester

Synonyms:N^α-(benzyloxycarbonyl)tryptophanyl-N^ε-(benzyloxycarbonyl)lysine methyl ester

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Chemical Property of N^α-(benzyloxycarbonyl)tryptophanyl-N^ε-(benzyloxycarbonyl)lysine methyl ester

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Technology Process of N^α-(benzyloxycarbonyl)tryptophanyl-N^ε-(benzyloxycarbonyl)lysine methyl ester

There total 1 articles about N^α-(benzyloxycarbonyl)tryptophanyl-N^ε-(benzyloxycarbonyl)lysine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 27894-50-4
methyl (2S)-2-amino-6-{[(benzyloxy)carbonyl]amino}hexanoate hydrochloride

: 7432-21-5
N-carbobenzyloxy-L-tryptophane

: 111237-83-3
N^α-(benzyloxycarbonyl)tryptophanyl-N^ε-(benzyloxycarbonyl)lysine methyl ester

Guidance literature:: With triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; for 2h; Ambient temperature;
DOI:10.1021/jm00397a004

Reference yield: 82.0%

: 7669-54-7
2-nitrobenzenesulfenyl chloride

: 111237-83-3
N^α-(benzyloxycarbonyl)tryptophanyl-N^ε-(benzyloxycarbonyl)lysine methyl ester

: 111237-91-3
N^α-(benzyloxycarbonyl)-2-<(o-nitrophenyl)sulfenyl>tryptophanyl-N^ε-(benzyloxycarbonyl)lysine methyl ester

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; for 0.5h; Ambient temperature;
DOI:10.1021/jm00397a004

Reference yield:

: 111237-83-3
N^α-(benzyloxycarbonyl)tryptophanyl-N^ε-(benzyloxycarbonyl)lysine methyl ester

: 139091-29-5
Trp(Nps)-Lys-OMe

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / 1 N HCl / dioxane / 0.5 h / Ambient temperature

2: 61 percent / boron-tris(trifluoroacetate) / trifluoroacetic acid / 20 h / Ambient temperature

With hydrogenchloride; tris(trifluoro acetyloxy)borane; In 1,4-dioxane; trifluoroacetic acid;
DOI:10.1021/jm00397a004