C₅₅H₅₇NO₃S₂

Base Information

• Chemical Name: C₅₅H₅₇NO₃S₂
• CAS No.: 1353683-42-7
• Molecular Formula: C₅₅H₅₇NO₃S₂
• Molecular Weight: 844.194
• Mol file: 1353683-42-7.mol

Synonyms:C₅₅H₅₇NO₃S₂

Chemical Property of C₅₅H₅₇NO₃S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₅H₅₇NO₃S₂

There total 4 articles about C₅₅H₅₇NO₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C57H61NO4S2 → C55H57NO3S2 (1353683-42-7)

Guidance literature:

With acetic acid; In tetrahydrofuran; water; at 60 ℃;

DOI:10.1039/c1cc16248a

Reference yield:

4,16-dibromo[2.2]paracyclophane (196316-30-0,196316-31-1,23927-40-4,96392-77-7) → C55H57NO3S2 (1353683-42-7)

Guidance literature:

Multi-step reaction with 3 steps

1: trans-bis(triphenylphosphine)palladium dichloride / N,N-dimethyl-formamide / 12 h / 90 °C / Inert atmosphere

2: trans-bis(triphenylphosphine)palladium dichloride / N,N-dimethyl-formamide / 12 h / 90 °C / Inert atmosphere

3: acetic acid / tetrahydrofuran; water / 60 °C

With trans-bis(triphenylphosphine)palladium dichloride; acetic acid; In tetrahydrofuran; water; N,N-dimethyl-formamide; 1: Stille coupling / 2: Stille coupling;

DOI:10.1039/c1cc16248a

Reference yield:

C50H54BrNO2S (1353683-39-2) → C55H57NO3S2 (1353683-42-7)

Guidance literature:

Multi-step reaction with 2 steps

1: trans-bis(triphenylphosphine)palladium dichloride / N,N-dimethyl-formamide / 12 h / 90 °C / Inert atmosphere

2: acetic acid / tetrahydrofuran; water / 60 °C

With trans-bis(triphenylphosphine)palladium dichloride; acetic acid; In tetrahydrofuran; water; N,N-dimethyl-formamide; 1: Stille coupling;

DOI:10.1039/c1cc16248a

upstream raw materials:

C₅₀H₅₄BrNO₂S

[2.2]Paracyclophan

4,16-dibromo[2.2]paracyclophane