N,N-bis[(6-phenyl-2-pyridyl)methyl]-2-phenethylamine

Base Information

Chemical Name:N,N-bis[(6-phenyl-2-pyridyl)methyl]-2-phenethylamine
CAS No.:921625-96-9
Molecular Formula:C₃₂H₂₉N₃
Molecular Weight:455.602
Hs Code.:

Synonyms:N,N-bis[(6-phenyl-2-pyridyl)methyl]-2-phenethylamine

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Chemical Property of N,N-bis[(6-phenyl-2-pyridyl)methyl]-2-phenethylamine

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Technology Process of N,N-bis[(6-phenyl-2-pyridyl)methyl]-2-phenethylamine

There total 1 articles about N,N-bis[(6-phenyl-2-pyridyl)methyl]-2-phenethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 64-04-0
phenethylamine

: 157402-44-3
6-phenylpyridine-2-carbaldehyde

: 921625-96-9
N,N-bis[(6-phenyl-2-pyridyl)methyl]-2-phenethylamine

Guidance literature:: phenethylamine; 6-phenylpyridine-2-carbaldehyde; With acetic acid; In methanol; at 20 ℃; pH=4;

With sodium cyanoborohydride; In methanol; at 20 ℃;
DOI:10.1246/bcsj.79.1729

Reference yield: 51.0%

: 921625-96-9
N,N-bis[(6-phenyl-2-pyridyl)methyl]-2-phenethylamine

: 14057-91-1
tetrakis(acetonitrile)copper(I) perchlorate

: 75-05-8,26809-02-9
acetonitrile

: 921626-10-0
[Cu(N,N-bis[(6-phenyl-2-pyridyl)methyl]-2-phenethylamine)(CH₃CN)]ClO₄

Guidance literature:: In acetonitrile; (under Ar); ligand treated with soln. of Cu-complex in MeCN, stirred for5 min at room temp.; filtered, ether added, allowed to stand for several min, supernatant decanted, ppt. washed with ether, dried; elem. anal.;
DOI:10.1246/bcsj.79.1729

Reference yield:

: 921625-96-9
N,N-bis[(6-phenyl-2-pyridyl)methyl]-2-phenethylamine

: [Cu(N,N-bis[(6-phenyl-2-pyridyl)methyl]-2-phenethylamine)]ClO₄*0.67H₂O

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile

2: ethanol

3: methanol

In methanol; ethanol; acetonitrile;
DOI:10.1246/bcsj.79.1729