C₃₁H₃₅NO₆

Base Information

Chemical Name:C₃₁H₃₅NO₆
CAS No.:1359024-01-3
Molecular Formula:C₃₁H₃₅NO₆
Molecular Weight:517.622
Hs Code.:

C<sub>31</sub>H<sub>35</sub>NO<sub>6</sub>

Synonyms:C₃₁H₃₅NO₆

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Chemical Property of C₃₁H₃₅NO₆

Chemical Property:

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Technology Process of C₃₁H₃₅NO₆

There total 10 articles about C₃₁H₃₅NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1359022-59-5
phenyl 2-(benzyloxy)-4-bromo-6-methylbenzoate

: 85908-96-9
2-oxopiperidine-1-carboxylic acid tert-butyl ester

: 1359024-01-3
C₃₁H₃₅NO₆

Guidance literature:: phenyl 2-(benzyloxy)-4-bromo-6-methylbenzoate; With n-butyllithium; In tetrahydrofuran; hexanes; at -100 - -96 ℃;

2-oxopiperidine-1-carboxylic acid tert-butyl ester; In tetrahydrofuran; hexanes; at -92 - -78 ℃; for 1h;

With ammonium chloride; In tetrahydrofuran; hexanes; water; at 0 ℃;

Reference yield:

: 50868-73-0
2-methoxy-6-methylbenzeneamine

: 1359024-01-3
C₃₁H₃₅NO₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: bromine; acetic acid / methanol / 2 h / 20 °C / Cooling with ice

2.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 °C

2.2: 4 h / 0 - 50 °C

3.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / -78 - 20 °C

3.2: 1 h / 20 °C

4.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 20 °C

4.2: pH 1

5.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

6.1: triethylamine / dmap / 1 h / 20 °C

7.1: boron tribromide / dichloromethane / 0.58 h / -78 - 0 °C

7.2: 0.33 h / 20 °C

8.1: potassium carbonate / acetone / 20 °C

9.1: n-butyllithium / tetrahydrofuran; hexanes / -100 - -96 °C

9.2: 1 h / -92 - -78 °C

9.3: 0 °C

With hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; 2-methyl-but-2-ene; oxalyl dichloride; bromine; boron tribromide; diisobutylaluminium hydride; potassium carbonate; acetic acid; triethylamine; sodium nitrite; dmap; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; hexanes; dichloromethane; water; acetone; toluene; tert-butyl alcohol;

Reference yield:

: 877149-05-8
4-bromo-2-methoxy-6-methyl-benzonitrile

: 1359024-01-3
C₃₁H₃₅NO₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / -78 - 20 °C

1.2: 1 h / 20 °C

2.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 20 °C

2.2: pH 1

3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

4.1: triethylamine / dmap / 1 h / 20 °C

5.1: boron tribromide / dichloromethane / 0.58 h / -78 - 0 °C

5.2: 0.33 h / 20 °C

6.1: potassium carbonate / acetone / 20 °C

7.1: n-butyllithium / tetrahydrofuran; hexanes / -100 - -96 °C

7.2: 1 h / -92 - -78 °C

7.3: 0 °C

With sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; 2-methyl-but-2-ene; oxalyl dichloride; boron tribromide; diisobutylaluminium hydride; potassium carbonate; triethylamine; dmap; N,N-dimethyl-formamide; In tetrahydrofuran; hexanes; dichloromethane; water; acetone; toluene; tert-butyl alcohol;