methyl 6,7-anhydro-2,3-di-O-benzyl-4-O-carbamoyl-8-deoxy-α-D-threo-D-galacto-octoside

Base Information

Chemical Name:methyl 6,7-anhydro-2,3-di-O-benzyl-4-O-carbamoyl-8-deoxy-α-D-threo-D-galacto-octoside
CAS No.:131751-01-4
Molecular Formula:C₂₄H₂₉NO₇
Molecular Weight:443.497
Hs Code.:

Synonyms:methyl 6,7-anhydro-2,3-di-O-benzyl-4-O-carbamoyl-8-deoxy-α-D-threo-D-galacto-octoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 6,7-anhydro-2,3-di-O-benzyl-4-O-carbamoyl-8-deoxy-α-D-threo-D-galacto-octoside

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Technology Process of methyl 6,7-anhydro-2,3-di-O-benzyl-4-O-carbamoyl-8-deoxy-α-D-threo-D-galacto-octoside

There total 1 articles about methyl 6,7-anhydro-2,3-di-O-benzyl-4-O-carbamoyl-8-deoxy-α-D-threo-D-galacto-octoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124780-55-8
methyl 6,7-anhydro-2,3-di-O-benzyl-8-deoxy-α-D-threo-D-galacto-octopyranoside

: 3019-71-4
Trichloroacetyl isocyanate

: 131751-01-4
methyl 6,7-anhydro-2,3-di-O-benzyl-4-O-carbamoyl-8-deoxy-α-D-threo-D-galacto-octoside

Guidance literature:: With potassium carbonate; Yield given. Multistep reaction; 1.) THF, 5 min, 2.) THF, MeOH, overnight;
DOI:10.1071/CH9901657

Reference yield: 77.0%

: 131751-01-4
methyl 6,7-anhydro-2,3-di-O-benzyl-4-O-carbamoyl-8-deoxy-α-D-threo-D-galacto-octoside

: 124780-55-8
methyl 6,7-anhydro-2,3-di-O-benzyl-8-deoxy-α-D-threo-D-galacto-octopyranoside

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; for 2h; Heating;
DOI:10.1071/CH9901657

Reference yield:

: 131751-01-4
methyl 6,7-anhydro-2,3-di-O-benzyl-4-O-carbamoyl-8-deoxy-α-D-threo-D-galacto-octoside

: 131750-98-6
methyl 6,7-anhydro-2,3-di-O-benzyl-8-deoxy-4-O-methyl-α-D-threo-D-galacto-octoside

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / t-BuOK / tetrahydrofuran / 2 h / Heating

2: 1.) t-BuOK / 1.) THF, 5 min, 2.) 15 min

With potassium tert-butylate; In tetrahydrofuran;
DOI:10.1071/CH9901657