(Z)-N-benzylidene-1-(5-bromo-1H-indol-3-yl)-3-methylbutane-1-amine oxide

Base Information

Chemical Name:(Z)-N-benzylidene-1-(5-bromo-1H-indol-3-yl)-3-methylbutane-1-amine oxide
CAS No.:1309463-75-9
Molecular Formula:C₂₀H₂₁BrN₂O
Molecular Weight:385.304
Hs Code.:

Synonyms:(Z)-N-benzylidene-1-(5-bromo-1H-indol-3-yl)-3-methylbutane-1-amine oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-N-benzylidene-1-(5-bromo-1H-indol-3-yl)-3-methylbutane-1-amine oxide

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Technology Process of (Z)-N-benzylidene-1-(5-bromo-1H-indol-3-yl)-3-methylbutane-1-amine oxide

There total 3 articles about (Z)-N-benzylidene-1-(5-bromo-1H-indol-3-yl)-3-methylbutane-1-amine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1309463-59-9
N-benzyl-N-(1-(5-bromo-1H-indol-3-yl)-3-methylbutyl)-hydroxylamine

: 1309463-75-9
(Z)-N-benzylidene-1-(5-bromo-1H-indol-3-yl)-3-methylbutane-1-amine oxide

Guidance literature:: With manganese(IV) oxide; In toluene; at 100 ℃; for 0.0833333h;
DOI:10.1016/j.bmc.2011.03.060

Reference yield:

: 162365-56-2,162740-13-8
N-(3-methylbutylidene)benzylamine N-oxide

: 1309463-75-9
(Z)-N-benzylidene-1-(5-bromo-1H-indol-3-yl)-3-methylbutane-1-amine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; acetyl chloride / 2 h / 0 °C

2: manganese(IV) oxide / toluene / 0.08 h / 100 °C

With methanol; manganese(IV) oxide; acetyl chloride; In toluene;
DOI:10.1016/j.bmc.2011.03.060

Reference yield:

: 10075-50-0
5-bromo-1H-indole

: 1309463-75-9
(Z)-N-benzylidene-1-(5-bromo-1H-indol-3-yl)-3-methylbutane-1-amine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; acetyl chloride / 2 h / 0 °C

2: manganese(IV) oxide / toluene / 0.08 h / 100 °C

With methanol; manganese(IV) oxide; acetyl chloride; In toluene;
DOI:10.1016/j.bmc.2011.03.060