N(C₂H₅)4⁽¹⁺⁾*Re(C₅(CH₃)5)(CO)2(C₆F₅)^(1-) = [N(C₂H₅)4][Re(C₅(CH₃)5)(CO)2(C₆F₅)]

Base Information

Chemical Name:N(C₂H₅)4⁽¹⁺⁾*Re(C₅(CH₃)5)(CO)2(C₆F₅)^(1-) = [N(C₂H₅)4][Re(C₅(CH₃)5)(CO)2(C₆F₅)]
CAS No.:242816-72-4
Molecular Formula:C₈H₂₀N*C₁₈H₁₅F₅O₂Re
Molecular Weight:674.768
Hs Code.:

N(C<sub>2</sub>H<sub>5</sub>)4<sup>(1+)</sup>*Re(C<sub>5</sub>(CH<sub>3</sub>)5)(CO)2(C<sub>6</sub>F<sub>5</sub>)<sup>(1-)</sup> = [N(C<sub>2</sub>H<sub>5</sub>)4][Re(C<sub>5</sub>(CH<sub>3</sub>)5)(CO)2(C<sub>6</sub>F<sub>5</sub>)]

Synonyms:N(C₂H₅)4⁽¹⁺⁾*Re(C₅(CH₃)5)(CO)2(C₆F₅)^(1-) = [N(C₂H₅)4][Re(C₅(CH₃)5)(CO)2(C₆F₅)]

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Chemical Property of N(C₂H₅)4⁽¹⁺⁾*Re(C₅(CH₃)5)(CO)2(C₆F₅)^(1-) = [N(C₂H₅)4][Re(C₅(CH₃)5)(CO)2(C₆F₅)]

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Technology Process of N(C₂H₅)4⁽¹⁺⁾*Re(C₅(CH₃)5)(CO)2(C₆F₅)^(1-) = [N(C₂H₅)4][Re(C₅(CH₃)5)(CO)2(C₆F₅)]

There total 1 articles about N(C₂H₅)4⁽¹⁺⁾*Re(C₅(CH₃)5)(CO)2(C₆F₅)^(1-) = [N(C₂H₅)4][Re(C₅(CH₃)5)(CO)2(C₆F₅)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: {Re(η6-C5Me4CH2)(CO)2(C6F5)}

: 71-91-0
tetraethylammonium bromide

: 242816-72-4
N(C₂H₅)4⁽¹⁺⁾*Re(C₅(CH₃)5)(CO)2(C₆F₅)^(1-) = [N(C₂H₅)4][Re(C₅(CH₃)5)(CO)2(C₆F₅)]

Guidance literature:: With NaBH₄; In tetrahydrofuran; (N2); stirring (room temp., 30 min); solvent removal (vac.), dissoln. (CH2Cl2), filtration, concn., addn. of hexane with stirring, filtration, washing (hexane(, dissoln. (CH2Cl2), crystn. by slow layering of hexane;

Reference yield: 95.0%

: 242816-72-4
N(C₂H₅)4⁽¹⁺⁾*Re(C₅(CH₃)5)(CO)2(C₆F₅)^(1-) = [N(C₂H₅)4][Re(C₅(CH₃)5)(CO)2(C₆F₅)]

: 242816-73-5
Re(C₅(CH₃)5)(CO)2(H)(C₆F₅)

Guidance literature:: With aq. HCl; In diethyl ether; dichloromethane; (N2), stirring (room temp., 5 min); solvent removal (vac.), addn. of Et2O, filtration, solvent removal;