2-[(1S,2S,3S,4R,5R)-6-benzyloxy-2-hydroxy-4-(4-methoxybenzyloxy)-1,3,5-trimethylhexyl]-6-ethyl-3,5-dimethyl-4H-4-pyranone

Base Information

• Chemical Name: 2-[(1S,2S,3S,4R,5R)-6-benzyloxy-2-hydroxy-4-(4-methoxybenzyloxy)-1,3,5-trimethylhexyl]-6-ethyl-3,5-dimethyl-4H-4-pyranone
• CAS No.: 1158302-72-7
• Molecular Formula: C₃₃H₄₄O₆
• Molecular Weight: 536.709

Synonyms:2-[(1S,2S,3S,4R,5R)-6-benzyloxy-2-hydroxy-4-(4-methoxybenzyloxy)-1,3,5-trimethylhexyl]-6-ethyl-3,5-dimethyl-4H-4-pyranone

Chemical Property of 2-[(1S,2S,3S,4R,5R)-6-benzyloxy-2-hydroxy-4-(4-methoxybenzyloxy)-1,3,5-trimethylhexyl]-6-ethyl-3,5-dimethyl-4H-4-pyranone

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Technology Process of 2-[(1S,2S,3S,4R,5R)-6-benzyloxy-2-hydroxy-4-(4-methoxybenzyloxy)-1,3,5-trimethylhexyl]-6-ethyl-3,5-dimethyl-4H-4-pyranone

There total 1 articles about 2-[(1S,2S,3S,4R,5R)-6-benzyloxy-2-hydroxy-4-(4-methoxybenzyloxy)-1,3,5-trimethylhexyl]-6-ethyl-3,5-dimethyl-4H-4-pyranone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

C35H48O7 (1158302-71-6) → 2-[(1S,2S,3S,4R,5R)-6-benzyloxy-2-hydroxy-4-(4-methoxybenzyloxy)-1,3,5-trimethylhexyl]-6-ethyl-3,5-dimethyl-4H-4-pyranone (1158302-72-7)

Guidance literature:

C₃₅H₄₈O₇; With chloro-trimethyl-silane; tetrabutylammomium bromide; In dichloromethane; at -10 ℃; for 14h;

With water; sodium hydrogencarbonate; In dichloromethane;

DOI:10.1016/j.tet.2008.12.049

Reference yield: 90.0%

2-[(1S,2S,3S,4R,5R)-6-benzyloxy-2-hydroxy-4-(4-methoxybenzyloxy)-1,3,5-trimethylhexyl]-6-ethyl-3,5-dimethyl-4H-4-pyranone (1158302-72-7) → 2-((2S,3S,4S,5R,6R)-3,7-dihydroxy-5-((4-methoxybenzyl)oxy)-4,6-dimethylheptan-2-yl)-6-ethyl-3,5-dimethyl-4H-pyran-4-one (275355-99-2)

Guidance literature:

With hydrogen; nickel; In ethanol; at 20 ℃; for 5h;

DOI:10.1016/j.tet.2008.12.049

upstream raw materials:

C₃₅H₄₈O₇

Downstream raw materials:

2-((2S,3S,4S,5R,6R)-3,7-dihydroxy-5-((4-methoxybenzyl)oxy)-4,6-dimethylheptan-2-yl)-6-ethyl-3,5-dimethyl-4H-pyran-4-one

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