t-butyloxycarbonyl-L-kynurenylglycyl-L-phenylalanine 2,4,6-trimethylbenzyl ester

Base Information

Chemical Name:t-butyloxycarbonyl-L-kynurenylglycyl-L-phenylalanine 2,4,6-trimethylbenzyl ester
CAS No.:74802-14-5
Molecular Formula:C₃₆H₄₄N₄O₇
Molecular Weight:644.768
Hs Code.:

Synonyms:t-butyloxycarbonyl-L-kynurenylglycyl-L-phenylalanine 2,4,6-trimethylbenzyl ester

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Chemical Property of t-butyloxycarbonyl-L-kynurenylglycyl-L-phenylalanine 2,4,6-trimethylbenzyl ester

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Technology Process of t-butyloxycarbonyl-L-kynurenylglycyl-L-phenylalanine 2,4,6-trimethylbenzyl ester

There total 6 articles about t-butyloxycarbonyl-L-kynurenylglycyl-L-phenylalanine 2,4,6-trimethylbenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 18635-59-1
Phe-OTmb*HCl

: 74802-13-4
t-butyloxycarbonyl-L-kynurenylglycine p-nitrophenyl ester

: 74802-14-5
t-butyloxycarbonyl-L-kynurenylglycyl-L-phenylalanine 2,4,6-trimethylbenzyl ester

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; for 48h; Ambient temperature;

Reference yield:

: 2922-83-0
L-kynurenine

: 74802-14-5
t-butyloxycarbonyl-L-kynurenylglycyl-L-phenylalanine 2,4,6-trimethylbenzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / triethylamine / H₂O; dioxane / 5 h

2: 1.) N-methylmorpholine, isobutyl chloroformate / 1.) acetonitrile, -15 deg C, 10 min, 2.) acetonitrile, from -15 deg C to RT, 3 h

3: 91 percent / triethylamine / dimethylformamide / 48 h / Ambient temperature

With 4-methyl-morpholine; triethylamine; isobutyl chloroformate; In 1,4-dioxane; water; N,N-dimethyl-formamide;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 74802-14-5
t-butyloxycarbonyl-L-kynurenylglycyl-L-phenylalanine 2,4,6-trimethylbenzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / H₂O; dioxane / 5 h

2: 1.) N-methylmorpholine, isobutyl chloroformate / 1.) acetonitrile, -15 deg C, 10 min, 2.) acetonitrile, from -15 deg C to RT, 3 h

3: 91 percent / triethylamine / dimethylformamide / 48 h / Ambient temperature

With 4-methyl-morpholine; triethylamine; isobutyl chloroformate; In 1,4-dioxane; water; N,N-dimethyl-formamide;