7-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)heptanamide

Base Information

Chemical Name:7-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)heptanamide
CAS No.:1384189-17-6
Molecular Formula:C₄₆H₄₉NO₆
Molecular Weight:711.898
Hs Code.:

Synonyms:7-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)heptanamide

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Chemical Property of 7-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)heptanamide

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Technology Process of 7-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)heptanamide

There total 2 articles about 7-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)heptanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1384189-16-5
7-(anthracen-9-yloxy)-N-((2S,3S)-1,3-dihydroxybutan-2-yl)heptanamide

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1384189-17-6
7-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)heptanamide

Guidance literature:: With pyridine; dmap; at 20 ℃; for 24h; Inert atmosphere; Darkness;
DOI:10.1021/ja304205m

Reference yield:

: 913627-88-0
7-(anthracen-9-yloxy)heptanoic acid

: 1384189-17-6
7-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)heptanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: PyBOP / N,N-dimethyl-formamide / 0.25 h / 20 °C / Inert atmosphere; Darkness

1.2: 40 h / 40 °C / Inert atmosphere; Darkness

2.1: pyridine; dmap / 24 h / 20 °C / Inert atmosphere; Darkness

With pyridine; dmap; PyBOP; In N,N-dimethyl-formamide;
DOI:10.1021/ja304205m

Reference yield: 59.0%

: 1384189-17-6
7-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)heptanamide

: 124482-92-4,89992-70-1
2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine

: 1384189-18-7
(2S,3S)-3-(7-(anthracen-9-yloxy)heptanamido)-4-(bis(4-methoxyphenyl)(phenyl)methoxy)butan-2-yl (2-cyanoethyl) diisopropylphosphoramidite

Guidance literature:: 7-(anthracen-9-yloxy)-N-((2S,3S)-1-(bis(4-methoxyphenyl)(phenyl)methoxy)-3-hydroxybutan-2-yl)heptanamide; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; Inert atmosphere; Darkness;

2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine; In dichloromethane; for 1h; Inert atmosphere; Darkness;

In dichloromethane; for 0.5h; Inert atmosphere; Darkness;
DOI:10.1021/ja304205m