pentafluorophenyl-3-((tert-butoxy)-N-(2-((pentafluorophenyl)oxycarbonyl)ethyl)carbonylamino)propanoate

Base Information

Chemical Name:pentafluorophenyl-3-((tert-butoxy)-N-(2-((pentafluorophenyl)oxycarbonyl)ethyl)carbonylamino)propanoate
CAS No.:391247-73-7
Molecular Formula:C₂₃H₁₇F₁₀NO₆
Molecular Weight:593.375
Hs Code.:

Synonyms:pentafluorophenyl-3-((tert-butoxy)-N-(2-((pentafluorophenyl)oxycarbonyl)ethyl)carbonylamino)propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pentafluorophenyl-3-((tert-butoxy)-N-(2-((pentafluorophenyl)oxycarbonyl)ethyl)carbonylamino)propanoate

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Technology Process of pentafluorophenyl-3-((tert-butoxy)-N-(2-((pentafluorophenyl)oxycarbonyl)ethyl)carbonylamino)propanoate

There total 4 articles about pentafluorophenyl-3-((tert-butoxy)-N-(2-((pentafluorophenyl)oxycarbonyl)ethyl)carbonylamino)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 143766-89-6
3,3’-((tert-butoxycarbonyl)azanediyl)dipropanoic acid

: 391247-73-7
pentafluorophenyl-3-((tert-butoxy)-N-(2-((pentafluorophenyl)oxycarbonyl)ethyl)carbonylamino)propanoate

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1021/ja0109186

Reference yield:

: 111-94-4
3,3'-Iminodipropionitrile

: 391247-73-7
pentafluorophenyl-3-((tert-butoxy)-N-(2-((pentafluorophenyl)oxycarbonyl)ethyl)carbonylamino)propanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / AcCl / 11 h / Heating

2: 1.06 g / CHCl₃ / 20 °C

3: 2 N aq. NaOH / tetrahydrofuran / 20 h / 20 °C

4: 8.0 g / EDCI / dimethylformamide / 24 h / 20 °C

With sodium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; acetyl chloride; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/ja0109186

Reference yield:

: 67363-88-6
methyl 3-((2-(methoxycarbonyl)ethyl)amino)propanoate hydrochloride

: 391247-73-7
pentafluorophenyl-3-((tert-butoxy)-N-(2-((pentafluorophenyl)oxycarbonyl)ethyl)carbonylamino)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.06 g / CHCl₃ / 20 °C

2: 2 N aq. NaOH / tetrahydrofuran / 20 h / 20 °C

3: 8.0 g / EDCI / dimethylformamide / 24 h / 20 °C

With sodium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/ja0109186