2,4,5-trichloro-4-trifluoropyriMidine

Base Information

• Chemical Name: 2,4,5-trichloro-4-trifluoropyriMidine
• CAS No.: 84737-23-5
• Molecular Formula: C₅Cl₃F₃N₂
• Molecular Weight: 251.423
• Mol file: 84737-23-5.mol

Synonyms:NSC 331274

Chemical Property of 2,4,5-trichloro-4-trifluoropyriMidine

Chemical Property:

• Vapor Pressure: 0.0269mmHg at 25°C
• Boiling Point: 254.9°Cat760mmHg
• PKA: -8.98±0.41(Predicted)
• Flash Point: 108°C
• PSA: 25.78000
• Density: 1.731g/cm³
• LogP: 3.45560
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

2,4,5-Trichloro-6-(trifluoromethyl)pyrimidine 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4,5-trichloro-4-trifluoropyriMidine

There total 2 articles about 2,4,5-trichloro-4-trifluoropyriMidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

5-Chloro-6-trifluoromethyluracil (85730-40-1) + N,N-dimethyl-aniline (121-69-7,77733-26-7) → 4,5-Dichloro-2-N-methylanilino-6-trifluoromethylpyrimidine (93669-53-5) + 2,4,5-Trichloro-6-trifluoromethylpyrimidine (84737-23-5)

Guidance literature:

With trichlorophosphate; for 3h; Heating;

Reference yield: 36.0%

5-Chloro-6-trifluoromethyluracil (85730-40-1) → 4,5-Dichloro-2-N-methylanilino-6-trifluoromethylpyrimidine (93669-53-5) + 2,4,5-Trichloro-6-trifluoromethylpyrimidine (84737-23-5)

Guidance literature:

With N,N-dimethyl-aniline; trichlorophosphate; for 3h; Heating;

Reference yield: 85.0%

2,4,5-Trichloro-6-trifluoromethylpyrimidine (84737-23-5) + N-methylaniline (100-61-8) → 2,5-Dichloro-4-N-methylanilino-6-trifluoromethylpyrimidine (93669-59-1)

Guidance literature:

In ethanol; for 3h; Ambient temperature;

upstream raw materials:

5-Chloro-6-trifluoromethyluracil

N,N-dimethyl-aniline

Downstream raw materials:

2,5-Dichloro-4-N-methylanilino-6-trifluoromethylpyrimidine

5-Chloro-2,4-bis(N-methylanilino)-6-trifluoromethylpyrimidine

4-N-Methylanilino-6-trifluoromethylpyrimidin-2-ol

5-Chloro-2-methoxy-4-N-methylanilino-6-trifluoromethylpyrimidine

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