1-(4-methylphenyl)-dispiro[azetidine((2,9'-fluorene)(3,9'-xanthene))]-4-one

Base Information

Chemical Name:1-(4-methylphenyl)-dispiro[azetidine((2,9'-fluorene)(3,9'-xanthene))]-4-one
CAS No.:1344727-66-7
Molecular Formula:C₃₄H₂₃NO₂
Molecular Weight:477.562
Hs Code.:

Synonyms:1-(4-methylphenyl)-dispiro[azetidine((2,9'-fluorene)(3,9'-xanthene))]-4-one

Suppliers and Price of 1-(4-methylphenyl)-dispiro[azetidine((2,9'-fluorene)(3,9'-xanthene))]-4-one

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Chemical Property of 1-(4-methylphenyl)-dispiro[azetidine((2,9'-fluorene)(3,9'-xanthene))]-4-one

Chemical Property:

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Technology Process of 1-(4-methylphenyl)-dispiro[azetidine((2,9'-fluorene)(3,9'-xanthene))]-4-one

There total 3 articles about 1-(4-methylphenyl)-dispiro[azetidine((2,9'-fluorene)(3,9'-xanthene))]-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 82-07-5
xanthene-9-carboxylic acid

: 10183-83-2
N-(9H-fluoren-9-ylidene)-4-methylaniline

: 1344727-66-7
1-(4-methylphenyl)-dispiro[azetidine((2,9'-fluorene)(3,9'-xanthene))]-4-one

Guidance literature:: With triethylamine; p-toluenesulfonyl chloride; In dichloromethane; at 20 ℃; for 15h;
DOI:10.1016/j.tet.2011.09.041

Reference yield:

: 486-25-9,952573-42-1
9-fluorenone

: 1344727-66-7
1-(4-methylphenyl)-dispiro[azetidine((2,9'-fluorene)(3,9'-xanthene))]-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / ethanol / 12 h / Reflux

2: triethylamine; p-toluenesulfonyl chloride / dichloromethane / 15 h / 20 °C

With acetic acid; triethylamine; p-toluenesulfonyl chloride; In ethanol; dichloromethane; 2: Staudinger reaction;
DOI:10.1016/j.tet.2011.09.041

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 1344727-66-7
1-(4-methylphenyl)-dispiro[azetidine((2,9'-fluorene)(3,9'-xanthene))]-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / ethanol / 12 h / Reflux

2: triethylamine; p-toluenesulfonyl chloride / dichloromethane / 15 h / 20 °C

With acetic acid; triethylamine; p-toluenesulfonyl chloride; In ethanol; dichloromethane; 2: Staudinger reaction;
DOI:10.1016/j.tet.2011.09.041