phenyl 5-(p-tolyl)tetrazol-2-yl ketone p-nitrophenylhydrazone

Base Information

• Chemical Name: phenyl 5-(p-tolyl)tetrazol-2-yl ketone p-nitrophenylhydrazone
• CAS No.: 117594-34-0
• Molecular Formula: C₂₁H₁₇N₇O₂
• Molecular Weight: 399.412
• Mol file: 117594-34-0.mol

Synonyms:phenyl 5-(p-tolyl)tetrazol-2-yl ketone p-nitrophenylhydrazone

Chemical Property of phenyl 5-(p-tolyl)tetrazol-2-yl ketone p-nitrophenylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenyl 5-(p-tolyl)tetrazol-2-yl ketone p-nitrophenylhydrazone

There total 1 articles about phenyl 5-(p-tolyl)tetrazol-2-yl ketone p-nitrophenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

5-(p-tolyl)-1H-tetrazole (24994-04-5) + N-(4-nitrophenyl)benzohydrazonoyl bromide (962-13-0) → phenyl 5-(p-tolyl)tetrazol-2-yl ketone p-nitrophenylhydrazone (117594-34-0) + phenyl 5-(p-tolyl)tetrazol-1-yl ketone p-nitrophenylhydrazone (117594-22-6)

Guidance literature:

With triethylamine; In benzene; for 3h; Product distribution; Heating; substituent effects on orientation of nitril imide attack on 5-aryl tetrazoles;

Reference yield: 89.0%

phenyl 5-(p-tolyl)tetrazol-2-yl ketone p-nitrophenylhydrazone (117594-34-0) → 4-(p-nitroanilino)-3-phenyl-5-(p-tolyl)-1,2,4-triazole (117594-49-7)

Guidance literature:

In various solvent(s); for 5h; Heating;

Reference yield: 78.0%

phenyl 5-(p-tolyl)tetrazol-2-yl ketone p-nitrophenylhydrazone (117594-34-0) → 1-(4-Nitro-phenyl)-3-phenyl-6-p-tolyl-1,4-dihydro-[1,2,4,5]tetrazine (136920-13-3)

Guidance literature:

With 3-chlorobenzoate; In various solvent(s); at 156 ℃; for 5h;

upstream raw materials:

5-(p-tolyl)-1H-tetrazole

N-(4-nitrophenyl)benzohydrazonoyl bromide

Downstream raw materials:

4-(p-nitroanilino)-3-phenyl-5-(p-tolyl)-1,2,4-triazole

1-(4-Nitro-phenyl)-3-phenyl-6-p-tolyl-1,4-dihydro-[1,2,4,5]tetrazine