3-(3,5-dimethylisoxazol-4-yl)-4-(4-hydroxyphenyl)thiophene-2-carbaldehyde oxime

Base Information

Chemical Name:3-(3,5-dimethylisoxazol-4-yl)-4-(4-hydroxyphenyl)thiophene-2-carbaldehyde oxime
CAS No.:1360604-75-6
Molecular Formula:C₁₆H₁₄N₂O₃S
Molecular Weight:314.365
Hs Code.:

Synonyms:3-(3,5-dimethylisoxazol-4-yl)-4-(4-hydroxyphenyl)thiophene-2-carbaldehyde oxime

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Chemical Property of 3-(3,5-dimethylisoxazol-4-yl)-4-(4-hydroxyphenyl)thiophene-2-carbaldehyde oxime

Chemical Property:

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Technology Process of 3-(3,5-dimethylisoxazol-4-yl)-4-(4-hydroxyphenyl)thiophene-2-carbaldehyde oxime

There total 3 articles about 3-(3,5-dimethylisoxazol-4-yl)-4-(4-hydroxyphenyl)thiophene-2-carbaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1360605-09-9
3-(3,5-dimethylisoxazol-4-yl)-4-(4-hydroxyphenyl)thiophene-2-carbaldehyde

: 1360604-75-6
3-(3,5-dimethylisoxazol-4-yl)-4-(4-hydroxyphenyl)thiophene-2-carbaldehyde oxime

Guidance literature:: With pyridine; hydroxylamine hydrochloride; In ethanol; at 150 ℃; for 0.166667h; Microwave irradiation;

Reference yield:

: 32896-02-9
3,4-dibromo thiophene-2-carboxaldehyde

: 1360604-75-6
3-(3,5-dimethylisoxazol-4-yl)-4-(4-hydroxyphenyl)thiophene-2-carbaldehyde oxime

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 0.33 h / 140 °C / Microwave irradiation

2: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 0.33 h / 140 °C / Microwave irradiation

3: hydroxylamine hydrochloride; pyridine / ethanol / 0.17 h / 150 °C / Microwave irradiation

With pyridine; hydroxylamine hydrochloride; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; toluene;

Reference yield:

: 1360605-08-8
4-bromo-3-(3,5-dimethylisoxazol-4-yl)thiophene-2-carbaldehyde

: 1360604-75-6
3-(3,5-dimethylisoxazol-4-yl)-4-(4-hydroxyphenyl)thiophene-2-carbaldehyde oxime

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 0.33 h / 140 °C / Microwave irradiation

2: hydroxylamine hydrochloride; pyridine / ethanol / 0.17 h / 150 °C / Microwave irradiation

With pyridine; hydroxylamine hydrochloride; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; toluene;