4-(3',4',5'-trimethoxyphenyl)-1-cyano-2-oxo-6,7-methylenedioxy-1,3,4,9-tetrahydro-1H-benzindene

Base Information

Chemical Name:4-(3',4',5'-trimethoxyphenyl)-1-cyano-2-oxo-6,7-methylenedioxy-1,3,4,9-tetrahydro-1H-benzindene
CAS No.:112182-83-9
Molecular Formula:C₂₄H₂₁NO₆
Molecular Weight:419.434
Hs Code.:

4-(3',4',5'-trimethoxyphenyl)-1-cyano-2-oxo-6,7-methylenedioxy-1,3,4,9-tetrahydro-1H-benz<f>indene

Synonyms:4-(3',4',5'-trimethoxyphenyl)-1-cyano-2-oxo-6,7-methylenedioxy-1,3,4,9-tetrahydro-1H-benzindene

Suppliers and Price of 4-(3',4',5'-trimethoxyphenyl)-1-cyano-2-oxo-6,7-methylenedioxy-1,3,4,9-tetrahydro-1H-benzindene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(3',4',5'-trimethoxyphenyl)-1-cyano-2-oxo-6,7-methylenedioxy-1,3,4,9-tetrahydro-1H-benzindene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(3',4',5'-trimethoxyphenyl)-1-cyano-2-oxo-6,7-methylenedioxy-1,3,4,9-tetrahydro-1H-benzindene

There total 5 articles about 4-(3',4',5'-trimethoxyphenyl)-1-cyano-2-oxo-6,7-methylenedioxy-1,3,4,9-tetrahydro-1H-benzindene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 112182-82-8
(R)-7-Imino-9-(3,4,5-trimethoxy-phenyl)-6,7,8,9-tetrahydro-5H-1,3-dioxa-dicyclopenta[b,g]naphthalene-6-carbonitrile

: 112182-83-9
4-(3',4',5'-trimethoxyphenyl)-1-cyano-2-oxo-6,7-methylenedioxy-1,3,4,9-tetrahydro-1H-benzindene

Guidance literature:: With hydrogenchloride; In ethanol; for 1h; Ambient temperature;

Reference yield:

: 104720-04-9
β-apopicropodophyllol

: 112182-83-9
4-(3',4',5'-trimethoxyphenyl)-1-cyano-2-oxo-6,7-methylenedioxy-1,3,4,9-tetrahydro-1H-benzindene

Guidance literature:: Multi-step reaction with 4 steps

1: 49 percent / pyridine / 48 h / 5 - 10 °C

2: dimethylsulfoxide / 1.5 h / 90 - 95 °C

3: sodium hydride / dimethylsulfoxide / 1 h / 90 - 95 °C

4: 79 percent / 6 M hydrochloric acid / ethanol / 1 h / Ambient temperature

With pyridine; hydrogenchloride; sodium hydride; In ethanol; dimethyl sulfoxide;

Reference yield:

: [(R)-7-Cyanomethyl-5-(3,4,5-trimethoxy-phenyl)-5,8-dihydro-naphtho[2,3-d][1,3]dioxol-6-yl]-acetonitrile

: 112182-83-9
4-(3',4',5'-trimethoxyphenyl)-1-cyano-2-oxo-6,7-methylenedioxy-1,3,4,9-tetrahydro-1H-benzindene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / dimethylsulfoxide / 1 h / 90 - 95 °C

2: 79 percent / 6 M hydrochloric acid / ethanol / 1 h / Ambient temperature

With hydrogenchloride; sodium hydride; In ethanol; dimethyl sulfoxide;