C₂₄H₂₃NO₄

Base Information Edit

Chemical Name:C₂₄H₂₃NO₄
CAS No.:1613707-74-6
Molecular Formula:C₂₄H₂₃NO₄
Molecular Weight:389.451
Hs Code.:
Mol file:1613707-74-6.mol

C<sub>24</sub>H<sub>23</sub>NO<sub>4</sub>

Synonyms:C₂₄H₂₃NO₄

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Chemical Property of C₂₄H₂₃NO₄ Edit

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Technology Process of C₂₄H₂₃NO₄

There total 4 articles about C₂₄H₂₃NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 3453-40-5
3-(6-methoxynaphthalen-2-yl)propionic acid

: 101711-90-4,123731-35-1,128677-61-2
(S)-4-benzyl-2-oxazolidinone lithium salt

: 1613707-74-6
C₂₄H₂₃NO₄

Guidance literature:: 3-(6-methoxynaphthalen-2-yl)propionic acid; With 4-methyl-morpholine; pivaloyl chloride; In tetrahydrofuran; at -78 ℃; for 0.0166667h;

(S)-4-benzyl-2-oxazolidinone lithium salt; In tetrahydrofuran; cyclohexane; at -78 - 20 ℃; for 1.17h;

Reference yield:

: 3453-33-6
6-methoxynaphthalene-2-carbaldehyde

: 1613707-74-6
C₂₄H₂₃NO₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / 0 °C

1.2: 16 h / 20 °C

2.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; ethyl acetate / 16 h / 20 °C / 760.05 Torr

3.1: water; sodium hydroxide / tetrahydrofuran; methanol / 2 h / 20 °C

4.1: 4-methyl-morpholine; pivaloyl chloride / tetrahydrofuran / 0.02 h / -78 °C

4.2: 1.17 h / -78 - 20 °C

With 4-methyl-morpholine; palladium 10% on activated carbon; water; hydrogen; pivaloyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate;

Reference yield:

: 136579-95-8
methyl 3-(6-methoxynaphthalen-2-yl)propanoate

: 1613707-74-6
C₂₄H₂₃NO₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; sodium hydroxide / tetrahydrofuran; methanol / 2 h / 20 °C

2.1: 4-methyl-morpholine; pivaloyl chloride / tetrahydrofuran / 0.02 h / -78 °C

2.2: 1.17 h / -78 - 20 °C

With 4-methyl-morpholine; water; pivaloyl chloride; sodium hydroxide; In tetrahydrofuran; methanol;