C₃₁H₃₈O₆

Base Information

Chemical Name:C₃₁H₃₈O₆
CAS No.:1320210-75-0
Molecular Formula:C₃₁H₃₈O₆
Molecular Weight:506.639
Hs Code.:

C<sub>31</sub>H<sub>38</sub>O<sub>6</sub>

Synonyms:C₃₁H₃₈O₆

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Chemical Property of C₃₁H₃₈O₆

Chemical Property:

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Technology Process of C₃₁H₃₈O₆

There total 8 articles about C₃₁H₃₈O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1320210-74-9
C₃₈H₄₂O₆

: 1320210-75-0
C₃₁H₃₈O₆

Guidance literature:: With methanol; 10-camphorsulfonic acid; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tet.2012.01.071

Reference yield:

: 1320210-69-2
C₂₂H₂₄O₅

: 1320210-75-0
C₃₁H₃₈O₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: benzene / 2 h / Inert atmosphere; Reflux

2.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.33 h / -78 °C / Inert atmosphere

3.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate / dichloromethane / Inert atmosphere; Molecular sieve

3.2: 10 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

4.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 6 h / -40 - 20 °C / Inert atmosphere

4.2: Saturated solution

5.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0 °C / Inert atmosphere

5.2: 19 h / 0 - 60 °C / Inert atmosphere

6.1: methanol; 10-camphorsulfonic acid / 24 h / 20 °C / Inert atmosphere

With titanium(IV) isopropylate; methanol; diethyl (2R,3R)-tartrate; sodium hydride; diisobutylaluminium hydride; 10-camphorsulfonic acid; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; benzene; 1.1: Wittig reaction / 3.1: Sharpless epoxidation / 3.2: Sharpless epoxidation;
DOI:10.1016/j.tet.2012.01.071

Reference yield:

: C₂₃H₂₆O₄

: 1320210-75-0
C₃₁H₃₈O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: ozone / methanol; dichloromethane / -78 °C

1.2: -78 - 20 °C

2.1: benzene / 2 h / Inert atmosphere; Reflux

3.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.33 h / -78 °C / Inert atmosphere

4.1: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate / dichloromethane / Inert atmosphere; Molecular sieve

4.2: 10 h / 0 - 20 °C / Inert atmosphere; Molecular sieve

5.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 6 h / -40 - 20 °C / Inert atmosphere

5.2: Saturated solution

6.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0 °C / Inert atmosphere

6.2: 19 h / 0 - 60 °C / Inert atmosphere

7.1: methanol; 10-camphorsulfonic acid / 24 h / 20 °C / Inert atmosphere

With titanium(IV) isopropylate; methanol; diethyl (2R,3R)-tartrate; sodium hydride; diisobutylaluminium hydride; ozone; 10-camphorsulfonic acid; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; benzene; 2.1: Wittig reaction / 4.1: Sharpless epoxidation / 4.2: Sharpless epoxidation;
DOI:10.1016/j.tet.2012.01.071