Technology Process of C34H35N3O4S
There total 12 articles about C34H35N3O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium phosphate / acetonitrile / 20 °C / Inert atmosphere
2: dimethyl sulfoxide / 20 °C / Inert atmosphere
3: water / 20 °C / Alkaline conditions; Inert atmosphere
With
potassium phosphate; water;
In
dimethyl sulfoxide; acetonitrile;
DOI:10.1021/jm3006788
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: potassium hydroxide / methanol; water / 21 h / 75 °C / Inert atmosphere
2.1: 20% Pd(OH)2/C; hydrogen / methanol / 18 h / 760.05 Torr / Inert atmosphere
3.1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere
3.2: 0 - 20 °C / Inert atmosphere
4.1: bromine; sodium acetate / Isopropyl acetate / 4 - 13 °C / Inert atmosphere
5.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate; lithium chloride / ethanol; water; toluene / 80 °C / Inert atmosphere
6.1: sodium hydroxide / tetrahydrofuran; methanol / Inert atmosphere
7.1: dimethyl sulfoxide / 20 °C / Inert atmosphere
8.1: water / 20 °C / Alkaline conditions; Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); 20% Pd(OH)2/C; water; hydrogen; bromine; sodium acetate; sodium carbonate; potassium carbonate; lithium chloride; potassium hydroxide; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol; Isopropyl acetate; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
5.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/jm3006788
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: potassium hydroxide / methanol; water / 21 h / 75 °C / Inert atmosphere
2.1: 20% Pd(OH)2/C; hydrogen / methanol / 18 h / 760.05 Torr / Inert atmosphere
3.1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere
3.2: 0 - 20 °C / Inert atmosphere
4.1: bromine; sodium acetate / Isopropyl acetate / 4 - 13 °C / Inert atmosphere
5.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate; lithium chloride / ethanol; water; toluene / 80 °C / Inert atmosphere
6.1: sodium hydroxide / tetrahydrofuran; methanol / Inert atmosphere
7.1: dimethyl sulfoxide / 20 °C / Inert atmosphere
8.1: water / 20 °C / Alkaline conditions; Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); 20% Pd(OH)2/C; water; hydrogen; bromine; sodium acetate; sodium carbonate; potassium carbonate; lithium chloride; potassium hydroxide; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol; Isopropyl acetate; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
5.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/jm3006788