(S)-5-((2-(2,2-dimethyl-1,3-dioxolan-4-yl)ethyl)thio)-1-phenyl-1H-tetrazole

Base Information

Chemical Name:(S)-5-((2-(2,2-dimethyl-1,3-dioxolan-4-yl)ethyl)thio)-1-phenyl-1H-tetrazole
CAS No.:860438-13-7
Molecular Formula:C₁₄H₁₈N₄O₂S
Molecular Weight:306.389
Hs Code.:

Synonyms:(S)-5-((2-(2,2-dimethyl-1,3-dioxolan-4-yl)ethyl)thio)-1-phenyl-1H-tetrazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-5-((2-(2,2-dimethyl-1,3-dioxolan-4-yl)ethyl)thio)-1-phenyl-1H-tetrazole

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Technology Process of (S)-5-((2-(2,2-dimethyl-1,3-dioxolan-4-yl)ethyl)thio)-1-phenyl-1H-tetrazole

There total 1 articles about (S)-5-((2-(2,2-dimethyl-1,3-dioxolan-4-yl)ethyl)thio)-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 32233-43-5
2-[(S)-2,2-dimethyl-1,3-dioxolan-4-yl]ethanol

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 860438-13-7
(S)-5-((2-(2,2-dimethyl-1,3-dioxolan-4-yl)ethyl)thio)-1-phenyl-1H-tetrazole

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine;
DOI:10.1016/j.tetlet.2011.01.086

Reference yield: 93.0%

: 860438-13-7
(S)-5-((2-(2,2-dimethyl-1,3-dioxolan-4-yl)ethyl)thio)-1-phenyl-1H-tetrazole

: 1227374-05-1
(S)-4-(1-phenyl-1H-tetrazol-5-ylthio)butane-1,2-diol

Guidance literature:: With acetyl chloride; In methanol; for 0.5h; Inert atmosphere;
DOI:10.1055/s-0029-1219376

Reference yield:

: 860438-13-7
(S)-5-((2-(2,2-dimethyl-1,3-dioxolan-4-yl)ethyl)thio)-1-phenyl-1H-tetrazole

: (E)-(R)-3-(tert-Butyl-diphenyl-silanyloxy)-6-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-hex-4-enoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 84 percent / Mo₇O₂₄(NH₄)6*4H₂O; aq. H₂O₂ / ethanol / 18 h / 20 °C

2.1: KHMDS / tetrahydrofuran; toluene / 4 h / -78 °C

2.2: 498 mg / PhSH; AIBN / benzene / 96 h / 90 °C

With ammonium molybdate tetrahydrate; dihydrogen peroxide; potassium hexamethylsilazane; In tetrahydrofuran; ethanol; toluene;
DOI:10.1021/ol0511833