3,5-bis(dibromomethyl)tetradeuteriobenzene

Base Information

• Chemical Name: 3,5-bis(dibromomethyl)tetradeuteriobenzene
• CAS No.: 477336-49-5
• Molecular Formula: C₈H₆Br₄
• Molecular Weight: 425.72
• Mol file: 477336-49-5.mol

Synonyms:3,5-bis(dibromomethyl)tetradeuteriobenzene

Chemical Property of 3,5-bis(dibromomethyl)tetradeuteriobenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,5-bis(dibromomethyl)tetradeuteriobenzene

There total 1 articles about 3,5-bis(dibromomethyl)tetradeuteriobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

tetradeutero-m-xylene (425420-97-9) → 3,5-bis(dibromomethyl)tetradeuteriobenzene (477336-49-5)

Guidance literature:

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; for 12h; Heating;

DOI:10.1021/ja012686g

Reference yield: 46.4%

3,5-bis(dibromomethyl)tetradeuteriobenzene (477336-49-5) → 2,4,5,6-tetradeuterioisophthalaldehyde (131170-43-9)

Guidance literature:

With 96 percent H₂SO₄; at 110 ℃;

DOI:10.1021/ja012686g

Reference yield:

3,5-bis(dibromomethyl)tetradeuteriobenzene (477336-49-5) → bis(1,3-propanedithioacetal) of 2,4,5,6-tetra-deuterioisophthalaldehyde (477336-50-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 46.4 percent / 96 percent H₂SO₄ / 110 °C

2: 84.2 percent / BF₃*Et₂O; AcOH / 264 h / 20 °C

With boron trifluoride diethyl etherate; acetic acid;

DOI:10.1021/ja012686g

upstream raw materials:

tetradeutero-m-xylene

Downstream raw materials:

2,4,5,6-tetradeuterioisophthalaldehyde

bis(1,3-propanedithioacetal) of 2,4,5,6-tetra-deuterioisophthalaldehyde