C₃₂H₅₄O₄Si₂

Base Information

Chemical Name:C₃₂H₅₄O₄Si₂
CAS No.:1591927-86-4
Molecular Formula:C₃₂H₅₄O₄Si₂
Molecular Weight:558.949
Hs Code.:

C<sub>32</sub>H<sub>54</sub>O<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₂H₅₄O₄Si₂

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Chemical Property of C₃₂H₅₄O₄Si₂

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Technology Process of C₃₂H₅₄O₄Si₂

There total 3 articles about C₃₂H₅₄O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1591927-49-9
C₃₂H₅₂O₄Si₂

: 1591927-86-4
C₃₂H₅₄O₄Si₂

Guidance literature:: With tetramethylammonium triacetoxyborohydride; In acetic acid; acetonitrile; at -40 - -30 ℃; for 24h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol5008179

Reference yield:

: 206255-62-1
4-(tert-butyl-dimethyl-silanyloxy)-3,3-dimethyl-butan-2-one

: 1591927-86-4
C₃₂H₅₄O₄Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / diethyl ether / 0 - 20 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / dichloromethane / -95 - -78 °C / Inert atmosphere

3: tetramethylammonium triacetoxyborohydride / acetonitrile; acetic acid / 24 h / -40 - -30 °C / Inert atmosphere

With boron trifluoride diethyl etherate; triethylamine; tetramethylammonium triacetoxyborohydride; In diethyl ether; dichloromethane; acetic acid; acetonitrile; 2: |Mukaiyama Aldol Addition;
DOI:10.1021/ol5008179

Reference yield:

: 1591927-46-6
C₁₅H₃₄O₂Si₂

: 1591927-86-4
C₃₂H₅₄O₄Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / dichloromethane / -95 - -78 °C / Inert atmosphere

2: tetramethylammonium triacetoxyborohydride / acetonitrile; acetic acid / 24 h / -40 - -30 °C / Inert atmosphere

With boron trifluoride diethyl etherate; tetramethylammonium triacetoxyborohydride; In dichloromethane; acetic acid; acetonitrile; 1: |Mukaiyama Aldol Addition;
DOI:10.1021/ol5008179