piperidine-1,4,4-tricarboxylic acid 1-tert-butyl 4,4-dibenzyl ester

Base Information

Chemical Name:piperidine-1,4,4-tricarboxylic acid 1-tert-butyl 4,4-dibenzyl ester
CAS No.:1093214-72-2
Molecular Formula:C₂₆H₃₁NO₆
Molecular Weight:453.535
Hs Code.:

Synonyms:piperidine-1,4,4-tricarboxylic acid 1-tert-butyl 4,4-dibenzyl ester

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Chemical Property of piperidine-1,4,4-tricarboxylic acid 1-tert-butyl 4,4-dibenzyl ester

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Technology Process of piperidine-1,4,4-tricarboxylic acid 1-tert-butyl 4,4-dibenzyl ester

There total 5 articles about piperidine-1,4,4-tricarboxylic acid 1-tert-butyl 4,4-dibenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5731-10-2
4'-fluoro-biphenyl-4-carboxylic acid

: 118753-70-1
N-(tert-butyloxycarbonyl)bis(2-chloroethyl)amine

: 1093214-72-2
piperidine-1,4,4-tricarboxylic acid 1-tert-butyl 4,4-dibenzyl ester

Guidance literature:: With potassium carbonate; tetrabutylammomium bromide; In toluene; for 6h; Heating / reflux;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1093214-72-2
piperidine-1,4,4-tricarboxylic acid 1-tert-butyl 4,4-dibenzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 2 h / 20 °C / pH 9 - 9.5

2: potassium carbonate / tetrabutylammomium bromide / toluene / 6 h / Heating / reflux

With potassium carbonate; triethylamine; tetrabutylammomium bromide; In dichloromethane; toluene;

Reference yield:

: 324-74-3
4-fluoro-biphenyl

: 1093214-72-2
piperidine-1,4,4-tricarboxylic acid 1-tert-butyl 4,4-dibenzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: aluminum (III) chloride / dichloromethane / 3 h / 5 - 20 °C

2.1: sodium hydroxide; potassium permanganate / tetrahydrofuran; water / 20 °C

2.2: pH ~ 2

3.1: potassium carbonate / tetrabutylammomium bromide / toluene / 6 h / Heating / reflux

With sodium hydroxide; potassium permanganate; potassium carbonate; aluminum (III) chloride; tetrabutylammomium bromide; In tetrahydrofuran; dichloromethane; water; toluene;