2-[3,5-di(thiophen-2-yl)phenyl]-9-(phenylsulfonyl)-9H-thieno-[2,3-b]carbazole

Base Information

Chemical Name:2-[3,5-di(thiophen-2-yl)phenyl]-9-(phenylsulfonyl)-9H-thieno-[2,3-b]carbazole
CAS No.:1273320-63-0
Molecular Formula:C₃₄H₂₁NO₂S₄
Molecular Weight:603.81
Hs Code.:

Synonyms:2-[3,5-di(thiophen-2-yl)phenyl]-9-(phenylsulfonyl)-9H-thieno-[2,3-b]carbazole

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Chemical Property of 2-[3,5-di(thiophen-2-yl)phenyl]-9-(phenylsulfonyl)-9H-thieno-[2,3-b]carbazole

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Technology Process of 2-[3,5-di(thiophen-2-yl)phenyl]-9-(phenylsulfonyl)-9H-thieno-[2,3-b]carbazole

There total 4 articles about 2-[3,5-di(thiophen-2-yl)phenyl]-9-(phenylsulfonyl)-9H-thieno-[2,3-b]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 15509-95-2
1,3,5-tris(2-thienyl)benzene

: 1273320-49-2
C₂₀H₁₈BrNO₆S

: 1273320-63-0
2-[3,5-di(thiophen-2-yl)phenyl]-9-(phenylsulfonyl)-9H-thieno-[2,3-b]carbazole

Guidance literature:: With zinc dibromide; In 1,2-dichloro-ethane; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1002/ejoc.201001309

Reference yield: 63.0%

: 1273320-61-8
2-[3,5-bis(3-methylthiophen-2-yl)phenyl]-3-methylthiophene

: 4-(2-(bromomethyl)-1-(phenylsulfonyl)-1H-indol-3-yl)but-3-en-2-one

: 1273320-63-0
2-[3,5-di(thiophen-2-yl)phenyl]-9-(phenylsulfonyl)-9H-thieno-[2,3-b]carbazole

Guidance literature:: With tin(IV) chloride; In 1,2-dichloro-ethane; at 20 ℃; Inert atmosphere;
DOI:10.1055/a-1387-9479

Reference yield:

: 1332607-78-9
[2-methyl-1-(phenylsulfonyl)-1H-indol-3-yl]methanediyl diacetate

: 1273320-63-0
2-[3,5-di(thiophen-2-yl)phenyl]-9-(phenylsulfonyl)-9H-thieno-[2,3-b]carbazole

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 1 h / Reflux

2: zinc dibromide / 1,2-dichloro-ethane / 4 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); zinc dibromide; In tetrachloromethane; 1,2-dichloro-ethane;
DOI:10.1002/ejoc.201001309