acetic acid 3-(4-cyanophenyl)-2-(4-cyanophenylazo)-2-methylpropyl ester

Base Information

Chemical Name:acetic acid 3-(4-cyanophenyl)-2-(4-cyanophenylazo)-2-methylpropyl ester
CAS No.:1268388-06-2
Molecular Formula:C₂₀H₁₈N₄O₂
Molecular Weight:346.389
Hs Code.:

Synonyms:acetic acid 3-(4-cyanophenyl)-2-(4-cyanophenylazo)-2-methylpropyl ester

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Chemical Property of acetic acid 3-(4-cyanophenyl)-2-(4-cyanophenylazo)-2-methylpropyl ester

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Technology Process of acetic acid 3-(4-cyanophenyl)-2-(4-cyanophenylazo)-2-methylpropyl ester

There total 1 articles about acetic acid 3-(4-cyanophenyl)-2-(4-cyanophenylazo)-2-methylpropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 820-71-3
methallyl acetate

: 2252-32-6
4-cyanophenyldiazonium tetrafluoroborate

: 1268388-06-2
acetic acid 3-(4-cyanophenyl)-2-(4-cyanophenylazo)-2-methylpropyl ester

Guidance literature:: With ferrous(II) sulfate heptahydrate; In water; dimethyl sulfoxide; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.11.137

Reference yield:

: 1268388-06-2
acetic acid 3-(4-cyanophenyl)-2-(4-cyanophenylazo)-2-methylpropyl ester

: (R)-4-((1-(4-cyanophenyl)-3-hydroxy-2-methylpropan-2-yl)diazenyl)benzonitrile

: (S)-4-((1-(4-cyanophenyl)-3-hydroxy-2-methylpropan-2-yl)diazenyl)benzonitrile

Guidance literature:: With lipase Candida antarctia B; In tert-butyl methyl ether; at 40 ℃; for 72h; pH=7.5; enantioselective reaction; Enzymatic reaction;
DOI:10.1016/j.tetlet.2010.11.137

Reference yield:

: 1268388-06-2
acetic acid 3-(4-cyanophenyl)-2-(4-cyanophenylazo)-2-methylpropyl ester

: (R)-4-((1-(4-cyanophenyl)-3-hydroxy-2-methylpropan-2-yl)diazenyl)benzonitrile

: (S)-4-((1-(4-cyanophenyl)-3-hydroxy-2-methylpropan-2-yl)diazenyl)benzonitrile

: (R)-acetic acid 3-(4-cyanophenyl)-2-(4-cyanophenylazo)-2-methylpropyl ester

: 1373396-11-2
(S)-acetic acid 3-(4-cyanophenyl)-2-(4-cyanophenylazo)-2-methylpropyl ester

Guidance literature:: With Candida antarctica lipase B; benzylamine; In acetonitrile; at 20 ℃; for 72h; optical yield given as %ee; Enzymatic reaction;
DOI:10.1039/c2ob25247c