[N'-(2,4-dinitro-phenyl)-hydrazino]-diphenyl-acetaldehyde-(2,4-dinitro-phenylhydrazone)

Base Information

• Chemical Name: [N'-(2,4-dinitro-phenyl)-hydrazino]-diphenyl-acetaldehyde-(2,4-dinitro-phenylhydrazone)
• CAS No.: 1065-02-7
• Molecular Formula: C₂₆H₂₀N₈O₈
• Molecular Weight: 572.494
• Mol file: 1065-02-7.mol

Synonyms:[N'-(2,4-dinitro-phenyl)-hydrazino]-diphenyl-acetaldehyde-(2,4-dinitro-phenylhydrazone)

Chemical Property of [N'-(2,4-dinitro-phenyl)-hydrazino]-diphenyl-acetaldehyde-(2,4-dinitro-phenylhydrazone)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [N'-(2,4-dinitro-phenyl)-hydrazino]-diphenyl-acetaldehyde-(2,4-dinitro-phenylhydrazone)

There total 4 articles about [N'-(2,4-dinitro-phenyl)-hydrazino]-diphenyl-acetaldehyde-(2,4-dinitro-phenylhydrazone) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Diphenylacetaldehyde (947-91-1) → [N'-(2,4-dinitro-phenyl)-hydrazino]-diphenyl-acetaldehyde-(2,4-dinitro-phenylhydrazone) (1065-02-7)

Guidance literature:

Multi-step reaction with 2 steps

1: SO₂Cl₂

2: bis-(2-methoxy-ethyl) ether

With sulfuryl dichloride; In diethylene glycol dimethyl ether;

DOI:10.1021/ja01082a029

Reference yield:

α-Chloro-diphenylacetaldehyde (950-15-2) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → [N'-(2,4-dinitro-phenyl)-hydrazino]-diphenyl-acetaldehyde-(2,4-dinitro-phenylhydrazone) (1065-02-7)

Guidance literature:

In diethylene glycol dimethyl ether;

DOI:10.1021/ja01082a029

Reference yield:

p-toluenesulfonyl chloride (98-59-9) → [N'-(2,4-dinitro-phenyl)-hydrazino]-diphenyl-acetaldehyde-(2,4-dinitro-phenylhydrazone) (1065-02-7)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine

2: OsO₄; diethyl ether; pyridine / Behandeln des Oxidationsprodukts mit wss. KOH und Mannit in CHCl₃ und Behandeln des Reaktionsprodukts mit <2,4-Dinitro-phenyl>-hydrazin und wss.-aethanol. H₂SO₄

With pyridine; osmium(VIII) oxide; diethyl ether;

DOI:10.1021/jo01117a012

upstream raw materials:

2,2-diphenylvinyl 4-methylbenzenesulfonate

α-Chloro-diphenylacetaldehyde

(2,4-dinitro-phenyl)-hydrazine

p-toluenesulfonyl chloride