Technology Process of C22H34N2O4S
There total 8 articles about C22H34N2O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 80 percent / hydrogen, aq. conc. HCl / PtO2 / ethanol / 24 h / 2280 Torr
2: 97 percent / KHCO3 / methanol / 96 h
3: 64 percent / NaH, 4 Angstroem molecular sieves / dimethylformamide / 1.5 h / 20 °C
4: O3 / CH2Cl2; methanol / 1 h
5: methanol / 0.67 h / Heating
With
hydrogenchloride; 4 A molecular sieve; hydrogen; sodium hydride; potassium hydrogencarbonate; ozone;
platinum(IV) oxide;
In
methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19870700324
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 91 percent / NaBH4 / methanol / 0.17 h
2: 80 percent / hydrogen, aq. conc. HCl / PtO2 / ethanol / 24 h / 2280 Torr
3: 97 percent / KHCO3 / methanol / 96 h
4: 64 percent / NaH, 4 Angstroem molecular sieves / dimethylformamide / 1.5 h / 20 °C
5: O3 / CH2Cl2; methanol / 1 h
6: methanol / 0.67 h / Heating
With
hydrogenchloride; sodium tetrahydroborate; 4 A molecular sieve; hydrogen; sodium hydride; potassium hydrogencarbonate; ozone;
platinum(IV) oxide;
In
methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19870700324
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 95 percent / H2 / 10 percent Pd/C / ethanol / 3 h / 2280 Torr
2: O3 / CH2Cl2; methanol / 1 h
3: methanol / 0.67 h / Heating
With
hydrogen; ozone;
palladium on activated charcoal;
In
methanol; ethanol; dichloromethane;
DOI:10.1002/hlca.19870700324
