2-(3-amino-2-methoxypyridin-4-yl)-2-(phenylthio)acetaldehyde dimethylacetal

Base Information

Chemical Name:2-(3-amino-2-methoxypyridin-4-yl)-2-(phenylthio)acetaldehyde dimethylacetal
CAS No.:259684-48-5
Molecular Formula:C₁₆H₂₀N₂O₃S
Molecular Weight:320.412
Hs Code.:

Synonyms:2-(3-amino-2-methoxypyridin-4-yl)-2-(phenylthio)acetaldehyde dimethylacetal

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Chemical Property of 2-(3-amino-2-methoxypyridin-4-yl)-2-(phenylthio)acetaldehyde dimethylacetal

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Technology Process of 2-(3-amino-2-methoxypyridin-4-yl)-2-(phenylthio)acetaldehyde dimethylacetal

There total 4 articles about 2-(3-amino-2-methoxypyridin-4-yl)-2-(phenylthio)acetaldehyde dimethylacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20265-38-7
3-amino-2-methoxypyridine

: 259684-48-5
2-(3-amino-2-methoxypyridin-4-yl)-2-(phenylthio)acetaldehyde dimethylacetal

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 4 h / -70 °C

2: 7.0 g / NaOMe / methanol; CH₂Cl₂ / 18 h / 20 °C

With sodium methylate; triethylamine; In methanol; dichloromethane; 1: Condensation / 2: Rearrangement;
DOI:10.1080/07328319908044619

Reference yield:

: C₁₆H₂₁N₂O₃S⁽¹⁺⁾*Cl^(1-)

: 259684-48-5
2-(3-amino-2-methoxypyridin-4-yl)-2-(phenylthio)acetaldehyde dimethylacetal

Guidance literature:: With sodium methylate; In methanol; dichloromethane; at 20 ℃; for 18h;
DOI:10.1080/07328319908044619

Reference yield:

: 99172-76-6
phenylmercaptoacetaldehyde dimethyl acetal

: 259684-48-5
2-(3-amino-2-methoxypyridin-4-yl)-2-(phenylthio)acetaldehyde dimethylacetal

Guidance literature:: Multi-step reaction with 3 steps

1: Cl₂ / CH₂Cl₂ / 0.17 h / -75 - -65 °C

2: Et₃N / CH₂Cl₂ / 4 h / -70 °C

3: 7.0 g / NaOMe / methanol; CH₂Cl₂ / 18 h / 20 °C

With sodium methylate; chlorine; triethylamine; In methanol; dichloromethane; 1: Chlorination / 2: Condensation / 3: Rearrangement;
DOI:10.1080/07328319908044619