(Z)-3-(3-((4-(tert-butoxy)-4-oxobutyl)carbamoyl)-4-hydroxyphenyl)-2-methoxyacrylic acid

Base Information

Chemical Name:(Z)-3-(3-((4-(tert-butoxy)-4-oxobutyl)carbamoyl)-4-hydroxyphenyl)-2-methoxyacrylic acid
CAS No.:1613623-89-4
Molecular Formula:C₁₉H₂₅NO₇
Molecular Weight:379.41
Hs Code.:

Synonyms:(Z)-3-(3-((4-(tert-butoxy)-4-oxobutyl)carbamoyl)-4-hydroxyphenyl)-2-methoxyacrylic acid

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Chemical Property of (Z)-3-(3-((4-(tert-butoxy)-4-oxobutyl)carbamoyl)-4-hydroxyphenyl)-2-methoxyacrylic acid

Chemical Property:

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Technology Process of (Z)-3-(3-((4-(tert-butoxy)-4-oxobutyl)carbamoyl)-4-hydroxyphenyl)-2-methoxyacrylic acid

There total 3 articles about (Z)-3-(3-((4-(tert-butoxy)-4-oxobutyl)carbamoyl)-4-hydroxyphenyl)-2-methoxyacrylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1613623-88-3
(Z)-tert-butyl 4-(5-(2,3-dimethoxy-3-oxoprop-1-en-1-yl)-2-hydroxybenzamido)butanoate

: 1613623-89-4
(Z)-3-(3-((4-(tert-butoxy)-4-oxobutyl)carbamoyl)-4-hydroxyphenyl)-2-methoxyacrylic acid

Guidance literature:: With sodium hydroxide; In ethanol; water; at 25 ℃; for 3h;
DOI:10.1002/anie.201400529

Reference yield:

: (Z)-5-(2,3-dimethoxy-3-oxoprop-1-en-1-yl)-2-hydroxybenzoic acid

: 1613623-89-4
(Z)-3-(3-((4-(tert-butoxy)-4-oxobutyl)carbamoyl)-4-hydroxyphenyl)-2-methoxyacrylic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: dicyclohexyl-carbodiimide; 1-hydroxy-pyrrolidine-2,5-dione / tetrahydrofuran / 12 h / 25 °C

1.2: 18 h / 25 °C

2.1: tetrahydrofuran / 14 h / 25 °C

3.1: sodium hydroxide / water; ethanol / 3 h / 25 °C

With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; ethanol; water;
DOI:10.1002/anie.201400529

Reference yield:

: 1613623-86-1
C₁₆H₁₉NO₇

: 1613623-89-4
(Z)-3-(3-((4-(tert-butoxy)-4-oxobutyl)carbamoyl)-4-hydroxyphenyl)-2-methoxyacrylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 14 h / 25 °C

2: sodium hydroxide / water; ethanol / 3 h / 25 °C

With sodium hydroxide; In tetrahydrofuran; ethanol; water;
DOI:10.1002/anie.201400529