tert-butyl 4-(3,4,5-tris(octadecyloxy)benzoyl)piperazine-1-carboxylate

Base Information

Chemical Name:tert-butyl 4-(3,4,5-tris(octadecyloxy)benzoyl)piperazine-1-carboxylate
CAS No.:1380432-97-2
Molecular Formula:C₇₀H₁₃₀N₂O₆
Molecular Weight:1095.81
Hs Code.:

Synonyms:tert-butyl 4-(3,4,5-tris(octadecyloxy)benzoyl)piperazine-1-carboxylate

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Chemical Property of tert-butyl 4-(3,4,5-tris(octadecyloxy)benzoyl)piperazine-1-carboxylate

Chemical Property:

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Technology Process of tert-butyl 4-(3,4,5-tris(octadecyloxy)benzoyl)piperazine-1-carboxylate

There total 4 articles about tert-butyl 4-(3,4,5-tris(octadecyloxy)benzoyl)piperazine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 188685-36-1
3,4,5-tris(n-octadecan-1-yloxy)benzoyl chloride

: 57260-71-6
1-t-Butoxycarbonylpiperazine

: 1380432-97-2
tert-butyl 4-(3,4,5-tris(octadecyloxy)benzoyl)piperazine-1-carboxylate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 40 ℃; for 11h;
DOI:10.1002/chem.201300655

Reference yield:

: 99-24-1
methyl galloate

: 1380432-97-2
tert-butyl 4-(3,4,5-tris(octadecyloxy)benzoyl)piperazine-1-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 80 °C

2: potassium hydroxide / ethanol; water / 3 h / Reflux

3: thionyl chloride / toluene; N,N-dimethyl-formamide / 1 h / 50 °C

4: triethylamine / dichloromethane / 11 h / 0 - 40 °C

With thionyl chloride; potassium carbonate; triethylamine; potassium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1002/chem.201300655

Reference yield:

: 188685-33-8
methyl [3,4,5-tris(n-octadecan-1-yloxy)]benzoate

: 1380432-97-2
tert-butyl 4-(3,4,5-tris(octadecyloxy)benzoyl)piperazine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / ethanol; water / 3 h / Reflux

2: thionyl chloride / toluene; N,N-dimethyl-formamide / 1 h / 50 °C

3: triethylamine / dichloromethane / 11 h / 0 - 40 °C

With thionyl chloride; triethylamine; potassium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1002/chem.201300655